4-<3-(1,1-dimethylethoxy)-3-oxopropyl>benzeneacetic acid phenylmethyl ester

Base Information

Chemical Name:4-<3-(1,1-dimethylethoxy)-3-oxopropyl>benzeneacetic acid phenylmethyl ester
CAS No.:127153-01-9
Molecular Formula:C₂₂H₂₆O₄
Molecular Weight:354.446
Hs Code.:

Synonyms:4-<3-(1,1-dimethylethoxy)-3-oxopropyl>benzeneacetic acid phenylmethyl ester

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Chemical Property of 4-<3-(1,1-dimethylethoxy)-3-oxopropyl>benzeneacetic acid phenylmethyl ester

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Technology Process of 4-<3-(1,1-dimethylethoxy)-3-oxopropyl>benzeneacetic acid phenylmethyl ester

There total 5 articles about 4-<3-(1,1-dimethylethoxy)-3-oxopropyl>benzeneacetic acid phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 100-39-0
benzyl bromide

: 127153-00-8
4-<3-(1,1-dimethylethoxy)-3-oxopropyl>benzeneacetic acid

: 127153-01-9
4-<3-(1,1-dimethylethoxy)-3-oxopropyl>benzeneacetic acid phenylmethyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 24h;
DOI:10.1021/jm00107a037

Reference yield:

: 1,1-dimethylethyl 4-(carboxymethyl)phenylpropanoate

: 100-39-0
benzyl bromide

: 127153-01-9
4-<3-(1,1-dimethylethoxy)-3-oxopropyl>benzeneacetic acid phenylmethyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide;

Reference yield:

: 127152-98-1
benzyl 2-(4-bromophenyl)acetate

: 127153-01-9
4-<3-(1,1-dimethylethoxy)-3-oxopropyl>benzeneacetic acid phenylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / Et₃N, bis(triphenylphosphine)palladium dichloride / dimethylformamide / 12 h / 75 °C

2: 86 percent / H₂ / 10percent Pd/C / ethanol / 3 h

3: 92 percent / K₂CO₃ / dimethylformamide / 24 h

With bis-triphenylphosphine-palladium(II) chloride; hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00107a037