3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-allofuranose

Base Information

Chemical Name:3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-allofuranose
CAS No.:180404-49-3
Molecular Formula:C₁₉H₂₆N₂O₅S
Molecular Weight:394.492
Hs Code.:

Synonyms:3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-allofuranose

Suppliers and Price of 3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-allofuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-allofuranose

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-allofuranose

There total 2 articles about 3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-allofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 103-72-0
phenyl isothiocyanate

: 16848-19-4
1,2,5,6-di-O-isopropylidene-3-deoxy-3-amino-α-D-glucofuranoside

: 180404-49-3
3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-allofuranose

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/0008-6215(96)00039-0

Reference yield: 83.0%

: 103-72-0
phenyl isothiocyanate

: 3-Amino-3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-allofuranose hydrochloride

: 180404-49-3
3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-allofuranose

Guidance literature:: In pyridine; at 20 ℃; for 15h;
DOI:10.1016/0008-6215(96)00039-0

Reference yield: 12.0%

: 108-24-7
acetic anhydride

: 180404-49-3
3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-allofuranose

: 3-acetamido-2,5,6-tri-O-acetyl-3-deoxy-N-phenyl-α-D-allofuranosylamine 1,3-(cyclic thiourea)

: 3-acetamido-2,4,6-tri-O-acetyl-3-deoxy-N-phenyl-α-D-allopyranosylamine 1,3-(cyclic thiourea)

Guidance literature:: 3-deoxy-1,2:5,6-di-O-isopropylidene-3-(3-phenylthioureido)-α-D-allofuranose; With sulfuric acid; In 1,4-dioxane; for 5h; Heating;

acetic anhydride; With pyridine; dmap;
DOI:10.1016/S0040-4020(98)00872-2