3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-succinic acid monoester

Base Information

Chemical Name:3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-succinic acid monoester
CAS No.:470480-97-8
Molecular Formula:C₂₇H₂₅N₃O₆
Molecular Weight:487.512
Hs Code.:

Synonyms:3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-succinic acid monoester

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Chemical Property of 3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-succinic acid monoester

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Technology Process of 3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-succinic acid monoester

There total 1 articles about 3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-succinic acid monoester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 108-30-5
succinic acid anhydride

: 237766-09-5
[3-(acridin-9-ylamino)-5-hydroxymethylphenyl]carbamic acidethyl ester

: 470480-97-8
3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-succinic acid monoester

Guidance literature:: With pyridine; dmap; at 85 - 90 ℃; for 12h;
DOI:10.1021/jm0200714

Reference yield: 53.0%

: 155791-66-5
N-[2-(dimethylamino)ethyl]-1-methyl-4-aminopyrrolo-2-carboxamide

: 470480-97-8
3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-succinic acid monoester

: N-[5-(2-dimethylamino-ethylcarbamoyl)-1-methyl-1H-pyrrol-3-yl]-succinamic acid 3-(acridin-9-ylamino)-5-ethoxycarbonylamino-benzyl ester

Guidance literature:: 3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-succinic acid monoester; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; In N,N-dimethyl-formamide; at -5 ℃; for 2h;

N-[2-(dimethylamino)ethyl]-1-methyl-4-aminopyrrolo-2-carboxamide; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1021/jm0200714

Reference yield: 49.0%

: 162934-64-7
C₁₆H₂₄N₆O₂

: 470480-97-8
3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-succinic acid monoester

: N-[2-(dimethylamino)ethyl]-1-methyl-4-[1-methyl-4-[[[3-(9-acridinylamino)-5-(ethoxycarbonylamino)benzyloxy]carbonylpropanoyl]amino]pyrrole-2-carboxamido]pyrrole-2-carboxamide

Guidance literature:: 3-(9-acridinylamino)-5-hydroxymethylaniline-ethylcarbamate-O-succinic acid monoester; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; In N,N-dimethyl-formamide; at -5 ℃; for 2h;

C₁₆H₂₄N₆O₂; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1021/jm0200714