N-(3S-2-tert-butoxycarbonyl-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-phenylalanine

Base Information

Chemical Name:N-(3S-2-tert-butoxycarbonyl-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-phenylalanine
CAS No.:1034535-58-4
Molecular Formula:C₂₄H₂₈N₂O₅
Molecular Weight:424.497
Hs Code.:

Synonyms:N-(3S-2-tert-butoxycarbonyl-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-phenylalanine

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Chemical Property of N-(3S-2-tert-butoxycarbonyl-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-phenylalanine

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Technology Process of N-(3S-2-tert-butoxycarbonyl-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-phenylalanine

There total 1 articles about N-(3S-2-tert-butoxycarbonyl-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-phenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 500213-34-3
(S)-tert-butyl 3-(((S)-1-methoxy-1-oxo-3-phenylpropan-2-yl)carbamoyl)-3,4-dihydroisoquinoline-2(1H)-carboxylate

: 1034535-58-4
N-(3S-2-tert-butoxycarbonyl-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-phenylalanine

Guidance literature:: (S)-tert-butyl 3-(((S)-1-methoxy-1-oxo-3-phenylpropan-2-yl)carbamoyl)-3,4-dihydroisoquinoline-2(1H)-carboxylate; With water; sodium hydroxide; In methanol; at 0 ℃; for 3h; under 750.075 Torr; pH=11; Inert atmosphere;

With potassium hydrogensulfate; water; In methanol; under 750.075 Torr; pH=2 - 7; Inert atmosphere;
DOI:10.1016/j.ejmech.2009.08.002

Reference yield: 93.0%

: 1034535-58-4
N-(3S-2-tert-butoxycarbonyl-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-phenylalanine

: 1034535-96-0
N-(3S-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-phenylalanine

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 0 - 20 ℃; under 750.075 Torr; Inert atmosphere;
DOI:10.1016/j.ejmech.2009.08.002