methyl 12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate

Base Information

Chemical Name:methyl 12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate
CAS No.:88939-80-4
Molecular Formula:C₂₇H₂₀N₂O₅S
Molecular Weight:484.532
Hs Code.:

Synonyms:methyl 12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate

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Chemical Property of methyl 12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate

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Technology Process of methyl 12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate

There total 6 articles about methyl 12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 88939-78-0
methyl cis-5,6,6a,11a-tetrahydro-12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate

: 88939-80-4
methyl 12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene; for 8h; Heating;
DOI:10.1016/S0040-4020(01)88612-9

Reference yield:

: 83-34-1
3-Methylindole

: 88939-80-4
methyl 12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaH/mineral oil / 1.) THF, 5 deg C, 15 min; 20 deg C, 15 min; reflux, 1 h; 2.) THF, 20 deg C, 1 h

2: 66 percent / SnCl₄ / CH₂Cl₂ / 2 h / -25 °C

3: 97 percent / molecular sieves / CH₂Cl₂ / 48 h / 20 °C

4: 89 percent / chlorobenzene / 2 h / 110 °C

5: 64 percent / DDQ / toluene / 8 h / Heating

With molecular sieve; tin(IV) chloride; sodium hydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; mineral oil; In dichloromethane; chlorobenzene; toluene;
DOI:10.1016/S0040-4020(01)88612-9

Reference yield:

: 88939-68-8
1-<(p-methoxyphenyl)sulfonyl>-3-methylindole

: 88939-80-4
methyl 12<(p-methoxyphenyl)sulfonyl>-11H-indolo<2,3-a>carbazole-11-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / SnCl₄ / CH₂Cl₂ / 2 h / -25 °C

2: 97 percent / molecular sieves / CH₂Cl₂ / 48 h / 20 °C

3: 89 percent / chlorobenzene / 2 h / 110 °C

4: 64 percent / DDQ / toluene / 8 h / Heating

With molecular sieve; tin(IV) chloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; chlorobenzene; toluene;
DOI:10.1016/S0040-4020(01)88612-9