O-3'-senecioyl α-bisabolol β-D-fucopyranoside

Base Information

Chemical Name:O-3'-senecioyl α-bisabolol β-D-fucopyranoside
CAS No.:1356133-36-2
Molecular Formula:C₂₆H₄₂O₆
Molecular Weight:450.616
Hs Code.:

Synonyms:O-3'-senecioyl α-bisabolol β-D-fucopyranoside

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Chemical Property of O-3'-senecioyl α-bisabolol β-D-fucopyranoside

Chemical Property:

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Technology Process of O-3'-senecioyl α-bisabolol β-D-fucopyranoside

There total 12 articles about O-3'-senecioyl α-bisabolol β-D-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 3350-78-5
3,3-Dimethylacryloyl chloride

: 79197-22-1
(2R,3R,4S,5R,6S)-2-methyl-6-{[(2S)-6-methyl-2-(4-methylcyclohex-3-en-1-yl)hept-5-en-2-yl]oxy}tetrahydro-2H-pyran-3,4,5-triol

: 1356133-36-2
O-3'-senecioyl α-bisabolol β-D-fucopyranoside

: C₃₁H₄₈O₇

Guidance literature:: With 2,4,6-trimethyl-pyridine; 4-methoxy-2-(N-methylimidazolyl)phenylboronic acid; In 1,4-dioxane; at 20 ℃; for 16h; Reagent/catalyst; regioselective reaction;
DOI:10.1248/cpb.c20-00834

Reference yield:

: 3350-78-5
3,3-Dimethylacryloyl chloride

: 79197-22-1
(2R,3R,4S,5R,6S)-2-methyl-6-{[(2S)-6-methyl-2-(4-methylcyclohex-3-en-1-yl)hept-5-en-2-yl]oxy}tetrahydro-2H-pyran-3,4,5-triol

: 1356133-36-2
O-3'-senecioyl α-bisabolol β-D-fucopyranoside

: C₂₆H₄₂O₆

: C₃₁H₄₈O₇

Guidance literature:: With 2,4,6-trimethyl-pyridine; 10H-dibenzo[b,e][1,4]oxaborinin-10-ol; In 1,4-dioxane; at 20 ℃; for 16h; Reagent/catalyst;
DOI:10.1248/cpb.c20-00834

Reference yield:

: 1146468-69-0
2,3,4-Tri-O-benzoyl-6-desoxy-α,β-D-galactopyranose

: 1356133-36-2
O-3'-senecioyl α-bisabolol β-D-fucopyranoside

: C₃₁H₄₈O₇

Guidance literature:: Multi-step reaction with 4 steps

1: caesium carbonate / dichloromethane / 18 h / 20 °C

2: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 2 h / -78 °C / Molecular sieve

3: water; sodium hydroxide / tetrahydrofuran; methanol / 1 h / 20 °C

4: 4-methoxy-2-(N-methylimidazolyl)phenylboronic acid; 2,4,6-trimethyl-pyridine / 1,4-dioxane / 16 h / 20 °C

With 2,4,6-trimethyl-pyridine; trimethylsilyl trifluoromethanesulfonate; 4-methoxy-2-(N-methylimidazolyl)phenylboronic acid; water; caesium carbonate; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;
DOI:10.1248/cpb.c20-00834