2-[6-(2-methoxybenzyl)pyridin-2-yl]-7,7-dimethyl-5,6,7,8-tetrahydroquinazoline

Base Information

Chemical Name:2-[6-(2-methoxybenzyl)pyridin-2-yl]-7,7-dimethyl-5,6,7,8-tetrahydroquinazoline
CAS No.:1373153-13-9
Molecular Formula:C₂₃H₂₅N₃O
Molecular Weight:359.471
Hs Code.:

Synonyms:2-[6-(2-methoxybenzyl)pyridin-2-yl]-7,7-dimethyl-5,6,7,8-tetrahydroquinazoline

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Chemical Property of 2-[6-(2-methoxybenzyl)pyridin-2-yl]-7,7-dimethyl-5,6,7,8-tetrahydroquinazoline

Chemical Property:

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Technology Process of 2-[6-(2-methoxybenzyl)pyridin-2-yl]-7,7-dimethyl-5,6,7,8-tetrahydroquinazoline

There total 2 articles about 2-[6-(2-methoxybenzyl)pyridin-2-yl]-7,7-dimethyl-5,6,7,8-tetrahydroquinazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1373153-51-5
2-(6-bromopyridin-2-yl)-7,7-dimethyl-5,6,7,8-tetrahydroquinazoline

: 312693-15-5
(2-methoxybenzyl)zinc(II) chloride

: 1373153-13-9
2-[6-(2-methoxybenzyl)pyridin-2-yl]-7,7-dimethyl-5,6,7,8-tetrahydroquinazoline

Guidance literature:: 2-(6-bromopyridin-2-yl)-7,7-dimethyl-5,6,7,8-tetrahydroquinazoline; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; Reflux;

(2-methoxybenzyl)zinc(II) chloride; In tetrahydrofuran; for 1h; Reflux;

Reference yield:

: 1246780-10-8
1-((dimethylamino)methylidene)-5,5-dimethylcyclohexan-2-one

: 1245806-87-4
6-bromopicolinimidamide hydrochloride

: 1373153-13-9
2-[6-(2-methoxybenzyl)pyridin-2-yl]-7,7-dimethyl-5,6,7,8-tetrahydroquinazoline

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 0.5 h / 20 °C

1.2: 2 h / Reflux

2.1: bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / Reflux

2.2: 1 h / Reflux

With sodium methylate; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; methanol;