O-2-(2-phenyl-1(Z)-propenyl)-2-(2-propynyl)-4-pentynyl S-methyl dithiocarbonate

Base Information

Chemical Name:O-2-(2-phenyl-1(Z)-propenyl)-2-(2-propynyl)-4-pentynyl S-methyl dithiocarbonate
CAS No.:133129-83-6
Molecular Formula:C₁₉H₂₀OS₂
Molecular Weight:328.499
Hs Code.:

Synonyms:O-2-(2-phenyl-1(Z)-propenyl)-2-(2-propynyl)-4-pentynyl S-methyl dithiocarbonate

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Chemical Property of O-2-(2-phenyl-1(Z)-propenyl)-2-(2-propynyl)-4-pentynyl S-methyl dithiocarbonate

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Technology Process of O-2-(2-phenyl-1(Z)-propenyl)-2-(2-propynyl)-4-pentynyl S-methyl dithiocarbonate

There total 4 articles about O-2-(2-phenyl-1(Z)-propenyl)-2-(2-propynyl)-4-pentynyl S-methyl dithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115476-97-6
(E)-ethyl 4-phenylpent-2-enoate

: 133129-83-6
O-2-(2-phenyl-1(Z)-propenyl)-2-(2-propynyl)-4-pentynyl S-methyl dithiocarbonate

Guidance literature:: Multi-step reaction with 4 steps

1: 1) LDA, HMPA / 1) THF, -78 deg C, 15 min, 2) THF, 20 min

2: 1) LDA, HMPA / 1) THF, -78 deg C, 15 min, 2) THF, 20 min

3: LiAlH₄ / diethyl ether

4: 1) NaH / 1) THF, room temp., 1.5 h, 2) 2 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; sodium hydride; lithium diisopropyl amide; In diethyl ether;
DOI:10.1021/jo00008a048

Reference yield:

: (Z)-4-Phenyl-2-prop-2-ynyl-pent-3-enoic acid ethyl ester

: 133129-83-6
O-2-(2-phenyl-1(Z)-propenyl)-2-(2-propynyl)-4-pentynyl S-methyl dithiocarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 1) LDA, HMPA / 1) THF, -78 deg C, 15 min, 2) THF, 20 min

2: LiAlH₄ / diethyl ether

3: 1) NaH / 1) THF, room temp., 1.5 h, 2) 2 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; sodium hydride; lithium diisopropyl amide; In diethyl ether;
DOI:10.1021/jo00008a048

Reference yield:

: 133129-98-3
(Z)-4-Phenyl-2,2-di-prop-2-ynyl-pent-3-enoic acid ethyl ester

: 133129-83-6
O-2-(2-phenyl-1(Z)-propenyl)-2-(2-propynyl)-4-pentynyl S-methyl dithiocarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether

2: 1) NaH / 1) THF, room temp., 1.5 h, 2) 2 h

With lithium aluminium tetrahydride; sodium hydride; In diethyl ether;
DOI:10.1021/jo00008a048