N⁴-benzoyl-3',5'-O-1,1,3,3-tetraisopropyldisiloxane-1,3-diyl[5-13C]cytidine

Base Information

Chemical Name:N⁴-benzoyl-3',5'-O-1,1,3,3-tetraisopropyldisiloxane-1,3-diyl[5-13C]cytidine
CAS No.:445433-94-3
Molecular Formula:C₂₈H₄₃N₃O₇Si₂
Molecular Weight:590.825
Hs Code.:

N<sup>4</sup>-benzoyl-3',5'-O-1,1,3,3-tetraisopropyldisiloxane-1,3-diyl[5-13C]cytidine

Synonyms:N⁴-benzoyl-3',5'-O-1,1,3,3-tetraisopropyldisiloxane-1,3-diyl[5-13C]cytidine

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Chemical Property of N⁴-benzoyl-3',5'-O-1,1,3,3-tetraisopropyldisiloxane-1,3-diyl[5-13C]cytidine

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Technology Process of N⁴-benzoyl-3',5'-O-1,1,3,3-tetraisopropyldisiloxane-1,3-diyl[5-13C]cytidine

There total 4 articles about N⁴-benzoyl-3',5'-O-1,1,3,3-tetraisopropyldisiloxane-1,3-diyl[5-13C]cytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54447-56-2
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-[5-13C]ribose

: 445433-94-3
N⁴-benzoyl-3',5'-O-1,1,3,3-tetraisopropyldisiloxane-1,3-diyl[5-13C]cytidine

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / trimethylsilyl trifluoromethanesulfonate / toluene / 80 °C

2: NaOH; pyridine / methanol; H₂O

3: 231 mg / pyridine

With pyridine; sodium hydroxide; trimethylsilyl trifluoromethanesulfonate; In methanol; water; toluene;
DOI:10.1021/jo016281q

Reference yield:

: 184000-83-7
methyl 2,3,5-tri-O-benzoyl-D-[5-13C]ribofuranoside

: 445433-94-3
N⁴-benzoyl-3',5'-O-1,1,3,3-tetraisopropyldisiloxane-1,3-diyl[5-13C]cytidine

Guidance literature:: Multi-step reaction with 4 steps

1: H₂SO₄; AcOH / 3 h / 0 °C

2: 96 percent / trimethylsilyl trifluoromethanesulfonate / toluene / 80 °C

3: NaOH; pyridine / methanol; H₂O

4: 231 mg / pyridine

With pyridine; sodium hydroxide; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; acetic acid; In methanol; water; toluene;
DOI:10.1021/jo016281q

Reference yield:

: 184000-87-1
tetra-N⁴,O^2',O^3',O^5'-benzoyl[5'-13C]cytidine

: 445433-94-3
N⁴-benzoyl-3',5'-O-1,1,3,3-tetraisopropyldisiloxane-1,3-diyl[5-13C]cytidine

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH; pyridine / methanol; H₂O

2: 231 mg / pyridine

With pyridine; sodium hydroxide; In methanol; water;
DOI:10.1021/jo016281q