N-(2,3-dihydro-1H-inden-4-yl)-4-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

Base Information

Chemical Name:N-(2,3-dihydro-1H-inden-4-yl)-4-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide
CAS No.:913067-78-4
Molecular Formula:C₂₃H₂₈BNO₃
Molecular Weight:377.291
Hs Code.:

Synonyms:N-(2,3-dihydro-1H-inden-4-yl)-4-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

Suppliers and Price of N-(2,3-dihydro-1H-inden-4-yl)-4-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N-(2,3-dihydro-1H-inden-4-yl)-4-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(2,3-dihydro-1H-inden-4-yl)-4-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

There total 3 articles about N-(2,3-dihydro-1H-inden-4-yl)-4-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 913067-79-5
N-(2,3-dihydro-1H-inden-4-yl)-3-iodo-4-methylbenzamide

: 73183-34-3
bis(pinacol)diborane

: 913067-78-4
N-(2,3-dihydro-1H-inden-4-yl)-4-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In N,N-dimethyl-formamide; at 80 ℃; for 8h;
DOI:10.1021/jm0605482

Reference yield:

: 32202-61-2
4-aminoindan

: 913067-78-4
N-(2,3-dihydro-1H-inden-4-yl)-4-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 16.5 h / 20 °C

2: KOAc; Pd(dppf)Cl₂*CH₂Cl₂ / dimethylformamide / 8 h / 80 °C

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0605482

Reference yield:

: 52107-98-9
3-iodo-4-methylbenzoyl chloride

: 913067-78-4
N-(2,3-dihydro-1H-inden-4-yl)-4-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 16.5 h / 20 °C

2: KOAc; Pd(dppf)Cl₂*CH₂Cl₂ / dimethylformamide / 8 h / 80 °C

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0605482