E-1-formyl-2-(2-phenylpropenyl)cyclohexene tosylhyrazone

Base Information

Chemical Name:E-1-formyl-2-(2-phenylpropenyl)cyclohexene tosylhyrazone
CAS No.:94223-11-7
Molecular Formula:C₂₃H₂₆N₂O₂S
Molecular Weight:394.538
Hs Code.:

Synonyms:E-1-formyl-2-(2-phenylpropenyl)cyclohexene tosylhyrazone

Suppliers and Price of E-1-formyl-2-(2-phenylpropenyl)cyclohexene tosylhyrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of E-1-formyl-2-(2-phenylpropenyl)cyclohexene tosylhyrazone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of E-1-formyl-2-(2-phenylpropenyl)cyclohexene tosylhyrazone

There total 5 articles about E-1-formyl-2-(2-phenylpropenyl)cyclohexene tosylhyrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 94223-39-9
E-1-formyl-2-(2-phenylpropenyl)cyclohexene

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 94223-11-7
E-1-formyl-2-(2-phenylpropenyl)cyclohexene tosylhyrazone

Guidance literature:: With hydrogenchloride; In ethanol; at 35 - 40 ℃;
DOI:10.1016/S0040-4020(01)82434-0

Reference yield:

: 38127-47-8
2-bromocyclohex-1-ene-1-carbaldehyde

: 94223-11-7
E-1-formyl-2-(2-phenylpropenyl)cyclohexene tosylhyrazone

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / n-butyl lithium / diethyl ether / 1.) 0 deg C 2.) R_.T_., 1 h 3.) 0 deg C, 1 h 4.) R_.T_., 2 h 5.) reflux, 1 h

2: 58 percent / n-butyl lithium / tetrahydrofuran / -78 °C / 1.) 30 min 2.) 4 h

3: 84 percent / cc. HCl / ethanol / 35 - 40 °C

With hydrogenchloride; n-butyllithium; In tetrahydrofuran; diethyl ether; ethanol;
DOI:10.1016/S0040-4020(01)82434-0

Reference yield:

: 30537-09-8
(1-phenylethyl)triphenylphosphonium bromide

: 94223-11-7
E-1-formyl-2-(2-phenylpropenyl)cyclohexene tosylhyrazone

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / n-butyl lithium / diethyl ether / 1.) 0 deg C 2.) R_.T_., 1 h 3.) 0 deg C, 1 h 4.) R_.T_., 2 h 5.) reflux, 1 h

2: 58 percent / n-butyl lithium / tetrahydrofuran / -78 °C / 1.) 30 min 2.) 4 h

3: 84 percent / cc. HCl / ethanol / 35 - 40 °C

With hydrogenchloride; n-butyllithium; In tetrahydrofuran; diethyl ether; ethanol;
DOI:10.1016/S0040-4020(01)82434-0