3-methoxy-2-(4-methoxybenzyloxy)-5-methylhex-5-enoic acid (1-methoxy-2-phenylethyl)amide

Base Information

Chemical Name:3-methoxy-2-(4-methoxybenzyloxy)-5-methylhex-5-enoic acid (1-methoxy-2-phenylethyl)amide
CAS No.:866454-49-1
Molecular Formula:C₂₅H₃₃NO₅
Molecular Weight:427.541
Hs Code.:

Synonyms:3-methoxy-2-(4-methoxybenzyloxy)-5-methylhex-5-enoic acid (1-methoxy-2-phenylethyl)amide

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Chemical Property of 3-methoxy-2-(4-methoxybenzyloxy)-5-methylhex-5-enoic acid (1-methoxy-2-phenylethyl)amide

Chemical Property:

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Technology Process of 3-methoxy-2-(4-methoxybenzyloxy)-5-methylhex-5-enoic acid (1-methoxy-2-phenylethyl)amide

There total 6 articles about 3-methoxy-2-(4-methoxybenzyloxy)-5-methylhex-5-enoic acid (1-methoxy-2-phenylethyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2S,3R)-3-Methoxy-2-(4-methoxy-benzyloxy)-5-methyl-hex-5-enoic acid [1-methoxy-2-phenyl-eth-(Z)-ylidene]-amide

: 866454-49-1
3-methoxy-2-(4-methoxybenzyloxy)-5-methylhex-5-enoic acid (1-methoxy-2-phenylethyl)amide

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 0 ℃; for 2h;
DOI:10.1021/ol051396s

Reference yield:

: 3-methoxy-2-(4-methoxybenzyloxy)-5-methylhex-5-enal

: 866454-49-1
3-methoxy-2-(4-methoxybenzyloxy)-5-methylhex-5-enoic acid (1-methoxy-2-phenylethyl)amide

Guidance literature:: Multi-step reaction with 4 steps

1: 2-methyl-2-butene; aq. NaClO₂; NaH₂PO₄*H₂O / 2-methyl-propan-2-ol / 0.5 h / 20 °C

2: SOCl₂; Et₃N / CH₂Cl₂ / 2 h / 0 - 20 °C

3: Et₃N / CH₂Cl₂ / 4 h / 0 - 20 °C

4: 61 mg / NaBH₄ / ethanol / 2 h / 0 °C

With sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; thionyl chloride; 2-methyl-but-2-ene; triethylamine; In ethanol; dichloromethane; tert-butyl alcohol;
DOI:10.1021/ol051396s

Reference yield:

: 866454-55-9
3-methoxy-2-(4-methoxybenzyloxy)-5-methylhex-5-en-1-ol

: 866454-49-1
3-methoxy-2-(4-methoxybenzyloxy)-5-methylhex-5-enoic acid (1-methoxy-2-phenylethyl)amide

Guidance literature:: Multi-step reaction with 5 steps

1: SO₃*Py; DMSO; Et₃N / 0.33 h

2: 2-methyl-2-butene; aq. NaClO₂; NaH₂PO₄*H₂O / 2-methyl-propan-2-ol / 0.5 h / 20 °C

3: SOCl₂; Et₃N / CH₂Cl₂ / 2 h / 0 - 20 °C

4: Et₃N / CH₂Cl₂ / 4 h / 0 - 20 °C

5: 61 mg / NaBH₄ / ethanol / 2 h / 0 °C

With sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; thionyl chloride; 2-methyl-but-2-ene; pyridine-SO₃ complex; dimethyl sulfoxide; triethylamine; In ethanol; dichloromethane; tert-butyl alcohol;
DOI:10.1021/ol051396s