2-(tetradecyl)hexadecyl 2,3,4-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactopyranoside

Base Information

Chemical Name:2-(tetradecyl)hexadecyl 2,3,4-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactopyranoside
CAS No.:195323-41-2
Molecular Formula:C₆₃H₉₈O₉Si
Molecular Weight:1027.55
Hs Code.:

Synonyms:2-(tetradecyl)hexadecyl 2,3,4-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactopyranoside

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Chemical Property of 2-(tetradecyl)hexadecyl 2,3,4-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactopyranoside

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Technology Process of 2-(tetradecyl)hexadecyl 2,3,4-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactopyranoside

There total 5 articles about 2-(tetradecyl)hexadecyl 2,3,4-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 98-88-4
benzoyl chloride

: 195323-40-1
(2R,3R,4S,5R,6R)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-6-(2-tetradecyl-hexadecyloxy)-tetrahydro-pyran-3,4,5-triol

: 195323-41-2
2-(tetradecyl)hexadecyl 2,3,4-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactopyranoside

Guidance literature:: In pyridine; Ambient temperature;
DOI:10.1080/07328309708006543

Reference yield:

: 158847-14-4
2-tetradecylhexadecan-1-ol

: 195323-41-2
2-(tetradecyl)hexadecyl 2,3,4-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / molecular sieves / CH₂Cl₂ / Ambient temperature

2: NaOMe / methanol / 1 h / Heating

3: 293 mg / pyridine; CH₂Cl₂ / 6 h / Ambient temperature

4: 98 percent / pyridine / Ambient temperature

With molecular sieve; sodium methylate; In pyridine; methanol; dichloromethane;
DOI:10.1080/07328309708006543

Reference yield:

: 86520-63-0
2,3,4,6-tetra-O-acetyl-α-galactopyranosyl trichloroacetimidate

: 195323-41-2
2-(tetradecyl)hexadecyl 2,3,4-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / molecular sieves / CH₂Cl₂ / Ambient temperature

2: NaOMe / methanol / 1 h / Heating

3: 293 mg / pyridine; CH₂Cl₂ / 6 h / Ambient temperature

4: 98 percent / pyridine / Ambient temperature

With molecular sieve; sodium methylate; In pyridine; methanol; dichloromethane;
DOI:10.1080/07328309708006543