(R)-N-methyl-3-azabicyclo[3,3,1]nonan-9-yl 2'-cyclopentyl-2'-hydroxy-2'-phenylacetate

Base Information

Chemical Name:(R)-N-methyl-3-azabicyclo[3,3,1]nonan-9-yl 2'-cyclopentyl-2'-hydroxy-2'-phenylacetate
CAS No.:230313-75-4
Molecular Formula:C₂₂H₃₁NO₃
Molecular Weight:357.493
Hs Code.:

Synonyms:(R)-N-methyl-3-azabicyclo[3,3,1]nonan-9-yl 2'-cyclopentyl-2'-hydroxy-2'-phenylacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-N-methyl-3-azabicyclo[3,3,1]nonan-9-yl 2'-cyclopentyl-2'-hydroxy-2'-phenylacetate

Chemical Property:

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Technology Process of (R)-N-methyl-3-azabicyclo[3,3,1]nonan-9-yl 2'-cyclopentyl-2'-hydroxy-2'-phenylacetate

There total 10 articles about (R)-N-methyl-3-azabicyclo[3,3,1]nonan-9-yl 2'-cyclopentyl-2'-hydroxy-2'-phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 860644-55-9
(-)-2'-cyclopentyl-2'-phenyl-2'-hydroxyacetic acid [N-(2,2,2-trichloroethoxyformyl)-3-aza-bicyclo[3.3.1]nonan-9-yl]ester (+)-N-p-tosylglutamic acid salt

: 230313-75-4
(R)-N-methyl-3-azabicyclo[3,3,1]nonan-9-yl 2'-cyclopentyl-2'-hydroxy-2'-phenylacetate

Guidance literature:: With potassium hydroxide; In diethyl ether;

Reference yield:

: 137-43-9
Cyclopentyl bromide

: 230313-75-4
(R)-N-methyl-3-azabicyclo[3,3,1]nonan-9-yl 2'-cyclopentyl-2'-hydroxy-2'-phenylacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropylamide / hexane; diethyl ether / 0.5 h / -60 °C

1.2: hexane; diethyl ether / 2 h / -60 °C

1.3: KOH / methanol; H₂O / 3 h / Heating

2.1: diethyl ether / 0.5 h / 20 °C

3.1: NaH / heptane / 3 h / Heating

With sodium hydride; lithium diisopropyl amide; In diethyl ether; hexane; n-heptane;
DOI:10.1081/SCC-200057293

Reference yield:

: (5R)-2,5-diphenyl-1,3-dioxolan-4-one

: 230313-75-4
(R)-N-methyl-3-azabicyclo[3,3,1]nonan-9-yl 2'-cyclopentyl-2'-hydroxy-2'-phenylacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropylamide / hexane; diethyl ether / 0.5 h / -60 °C

1.2: hexane; diethyl ether / 2 h / -60 °C

1.3: KOH / methanol; H₂O / 3 h / Heating

2.1: diethyl ether / 0.5 h / 20 °C

3.1: NaH / heptane / 3 h / Heating

With sodium hydride; lithium diisopropyl amide; In diethyl ether; hexane; n-heptane;
DOI:10.1081/SCC-200057293