(-)-2'-cyclopentyl-2'-phenyl-2'-hydroxyacetic acid [N-(2,2,2-trichloroethoxyformyl)-3-aza-bicyclo[3.3.1]nonan-9-yl]ester (+)-N-p-tosylglutamic acid salt

Base Information

Chemical Name:(-)-2'-cyclopentyl-2'-phenyl-2'-hydroxyacetic acid [N-(2,2,2-trichloroethoxyformyl)-3-aza-bicyclo[3.3.1]nonan-9-yl]ester (+)-N-p-tosylglutamic acid salt
CAS No.:860644-55-9
Molecular Formula:C₁₂H₁₅NO₆S*C₂₁H₂₉NO₃
Molecular Weight:644.786
Hs Code.:

Synonyms:(-)-2'-cyclopentyl-2'-phenyl-2'-hydroxyacetic acid [N-(2,2,2-trichloroethoxyformyl)-3-aza-bicyclo[3.3.1]nonan-9-yl]ester (+)-N-p-tosylglutamic acid salt

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Chemical Property of (-)-2'-cyclopentyl-2'-phenyl-2'-hydroxyacetic acid [N-(2,2,2-trichloroethoxyformyl)-3-aza-bicyclo[3.3.1]nonan-9-yl]ester (+)-N-p-tosylglutamic acid salt

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Technology Process of (-)-2'-cyclopentyl-2'-phenyl-2'-hydroxyacetic acid [N-(2,2,2-trichloroethoxyformyl)-3-aza-bicyclo[3.3.1]nonan-9-yl]ester (+)-N-p-tosylglutamic acid salt

There total 2 articles about (-)-2'-cyclopentyl-2'-phenyl-2'-hydroxyacetic acid [N-(2,2,2-trichloroethoxyformyl)-3-aza-bicyclo[3.3.1]nonan-9-yl]ester (+)-N-p-tosylglutamic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 895153-68-1
3-azabicyclo[3,3,1]nonan-9-yl 2'-cyclopentyl-2'-hydroxy-2'-phenylacetate

: 4816-80-2
N-tosyl-L-glutamic acid

: 860644-55-9
(-)-2'-cyclopentyl-2'-phenyl-2'-hydroxyacetic acid [N-(2,2,2-trichloroethoxyformyl)-3-aza-bicyclo[3.3.1]nonan-9-yl]ester (+)-N-p-tosylglutamic acid salt

Guidance literature:: In ethanol; at 20 - 50 ℃; Resolution of racemate;

Reference yield:

: 56-86-0,21675-62-7,23009-64-5,25104-13-6,84960-48-5,25513-46-6
L-glutamic acid

: 98-59-9
p-toluenesulfonyl chloride

: 860644-55-9
(-)-2'-cyclopentyl-2'-phenyl-2'-hydroxyacetic acid [N-(2,2,2-trichloroethoxyformyl)-3-aza-bicyclo[3.3.1]nonan-9-yl]ester (+)-N-p-tosylglutamic acid salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / 70 °C

1.2: 0 °C / pH ~ 3

2.1: ethanol / 20 - 50 °C / Resolution of racemate

With sodium hydroxide; In ethanol;