isopropyl N-phenyl sulfinamoyl ester

Base Information

• Chemical Name: isopropyl N-phenyl sulfinamoyl ester
• CAS No.: 97821-21-1
• Molecular Formula: C₉H₁₃NOS
• Molecular Weight: 183.274
• Mol file: 97821-21-1.mol

Synonyms:isopropyl N-phenyl sulfinamoyl ester

Chemical Property of isopropyl N-phenyl sulfinamoyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of isopropyl N-phenyl sulfinamoyl ester

There total 7 articles about isopropyl N-phenyl sulfinamoyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

isopropylsulfinyl chloride (34256-07-0) + aniline (62-53-3) → isopropyl N-phenyl sulfinamoyl ester (97821-21-1)

Guidance literature:

In diethyl ether;

DOI:10.1080/10426507.2010.508691

Reference yield: 91.0%

isopropyl chloride (75-29-6) + N-phenylsulfinylamine (222851-56-1) → isopropyl N-phenyl sulfinamoyl ester (97821-21-1)

Guidance literature:

With magnesium; In diethyl ether; for 0.0833333h;

DOI:10.1016/0584-8539(85)80022-2

Reference yield:

methyl i-propylsulfinate (52693-47-7) + aniline (62-53-3) → isopropyl N-phenyl sulfinamoyl ester (97821-21-1)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; at -78 ℃;

DOI:10.1055/s-2007-1000850

upstream raw materials:

isopropyl chloride

N-phenylsulfinylamine

methyl i-propylsulfinate

aniline

Downstream raw materials:

ZnBr₂*2(N-phenyl 2-propane sulfinamide)

ZnCl₂*2(N-phenyl 2-propane sulfinamide)

N-phenylpropane-2-sulfonamide

(±)-2-methyl-N-phenylpropane-2-sulfinamide