5-[4-(4-dodecyloxybenzoyl)-phenyl]-2-(4-hydroxyphenyl)-1,3,4-oxadiazole

Base Information

Chemical Name:5-[4-(4-dodecyloxybenzoyl)-phenyl]-2-(4-hydroxyphenyl)-1,3,4-oxadiazole
CAS No.:881649-30-5
Molecular Formula:C₃₃H₃₈N₂O₅
Molecular Weight:542.675
Hs Code.:

Synonyms:5-[4-(4-dodecyloxybenzoyl)-phenyl]-2-(4-hydroxyphenyl)-1,3,4-oxadiazole

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Chemical Property of 5-[4-(4-dodecyloxybenzoyl)-phenyl]-2-(4-hydroxyphenyl)-1,3,4-oxadiazole

Chemical Property:

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Technology Process of 5-[4-(4-dodecyloxybenzoyl)-phenyl]-2-(4-hydroxyphenyl)-1,3,4-oxadiazole

There total 5 articles about 5-[4-(4-dodecyloxybenzoyl)-phenyl]-2-(4-hydroxyphenyl)-1,3,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 881640-60-4
5-(4-benzyloxyphenyl)-2-[4-(4-dodecyloxybenzoyl)-phenyl]-1,3,4-oxadiazole

: 881649-30-5
5-[4-(4-dodecyloxybenzoyl)-phenyl]-2-(4-hydroxyphenyl)-1,3,4-oxadiazole

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1039/b503846d

Reference yield:

: 881639-99-2
5-(4-benzyloxyphenyl)-2-(4-hydroxyphenyl)-1,3,4-oxadiazole

: 881649-30-5
5-[4-(4-dodecyloxybenzoyl)-phenyl]-2-(4-hydroxyphenyl)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / N-ethyl-N'-dimethylaminopropylcarbodiimide hydrochloride; DMAP / tetrahydrofuran / 96 h / 20 °C

2: 89 percent / H₂ / Pd/C / tetrahydrofuran; ethanol

With dmap; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1039/b503846d

Reference yield:

: 881639-97-0
4-hydroxybenzoic acid N'-(4-benzyloxybenzoyl)-hydrazine

: 881649-30-5
5-[4-(4-dodecyloxybenzoyl)-phenyl]-2-(4-hydroxyphenyl)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / SOCl₂; pyridine / 4 h / Heating

2: 76 percent / N-ethyl-N'-dimethylaminopropylcarbodiimide hydrochloride; DMAP / tetrahydrofuran / 96 h / 20 °C

3: 89 percent / H₂ / Pd/C / tetrahydrofuran; ethanol

With pyridine; dmap; thionyl chloride; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1039/b503846d