5-(4-benzyloxyphenyl)-2-[4-(4-dodecyloxybenzoyl)-phenyl]-1,3,4-oxadiazole

Base Information

Chemical Name:5-(4-benzyloxyphenyl)-2-[4-(4-dodecyloxybenzoyl)-phenyl]-1,3,4-oxadiazole
CAS No.:881640-60-4
Molecular Formula:C₄₀H₄₄N₂O₅
Molecular Weight:632.8
Hs Code.:

Synonyms:5-(4-benzyloxyphenyl)-2-[4-(4-dodecyloxybenzoyl)-phenyl]-1,3,4-oxadiazole

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Chemical Property of 5-(4-benzyloxyphenyl)-2-[4-(4-dodecyloxybenzoyl)-phenyl]-1,3,4-oxadiazole

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Technology Process of 5-(4-benzyloxyphenyl)-2-[4-(4-dodecyloxybenzoyl)-phenyl]-1,3,4-oxadiazole

There total 4 articles about 5-(4-benzyloxyphenyl)-2-[4-(4-dodecyloxybenzoyl)-phenyl]-1,3,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 881639-99-2
5-(4-benzyloxyphenyl)-2-(4-hydroxyphenyl)-1,3,4-oxadiazole

: 2312-15-4
p-dodecyloxybenzoic acid

: 881640-60-4
5-(4-benzyloxyphenyl)-2-[4-(4-dodecyloxybenzoyl)-phenyl]-1,3,4-oxadiazole

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; at 20 ℃; for 96h;
DOI:10.1039/b503846d

Reference yield:

: 881639-97-0
4-hydroxybenzoic acid N'-(4-benzyloxybenzoyl)-hydrazine

: 881640-60-4
5-(4-benzyloxyphenyl)-2-[4-(4-dodecyloxybenzoyl)-phenyl]-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / SOCl₂; pyridine / 4 h / Heating

2: 76 percent / N-ethyl-N'-dimethylaminopropylcarbodiimide hydrochloride; DMAP / tetrahydrofuran / 96 h / 20 °C

With pyridine; dmap; thionyl chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran;
DOI:10.1039/b503846d

Reference yield:

: 881638-34-2
4-benzyloxybenzoic acid pentafluorophenyl ester

: 881640-60-4
5-(4-benzyloxyphenyl)-2-[4-(4-dodecyloxybenzoyl)-phenyl]-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / dimethylformamide / 48 h / 20 °C

2: 80 percent / SOCl₂; pyridine / 4 h / Heating

3: 76 percent / N-ethyl-N'-dimethylaminopropylcarbodiimide hydrochloride; DMAP / tetrahydrofuran / 96 h / 20 °C

With pyridine; dmap; thionyl chloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/b503846d