N-cyclohexyl-N-[3-(4-nitrophenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide

Base Information

Chemical Name:N-cyclohexyl-N-[3-(4-nitrophenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide
CAS No.:698973-54-5
Molecular Formula:C₂₁H₂₆N₂O₃Si
Molecular Weight:382.535
Hs Code.:

Synonyms:N-cyclohexyl-N-[3-(4-nitrophenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide

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Chemical Property of N-cyclohexyl-N-[3-(4-nitrophenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide

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Technology Process of N-cyclohexyl-N-[3-(4-nitrophenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide

There total 4 articles about N-cyclohexyl-N-[3-(4-nitrophenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 636-98-6
p-nitrobenzene iodide

: 698973-51-2
N-cyclohexyl-N-(2-propynyl)-3-trimethylsilyl-2-propynamide

: 698973-54-5
N-cyclohexyl-N-[3-(4-nitrophenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide

Guidance literature:: With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; at 20 ℃; for 0.5h;

Reference yield:

: 3173-53-3
Cyclohexyl isocyanate

: 698973-54-5
N-cyclohexyl-N-[3-(4-nitrophenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 0.08 h / -78 °C

1.2: tetrahydrofuran; hexane / 0.33 h / -78 °C

2.1: 2.48 g / tetrahydrofuran; hexane / 60 h / 20 °C

3.1: 86 percent / CuI; Et₃N / PdCl₂(PPh₃)2 / tetrahydrofuran / 0.5 h / 20 °C

With copper(l) iodide; n-butyllithium; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; hexane;

Reference yield:

: 910807-83-9
3-Trimethylsilanyl-propynoic acid cyclohexylamide

: 698973-54-5
N-cyclohexyl-N-[3-(4-nitrophenyl)-2-propynyl]-3-trimethylsilyl-2-propynamide

Guidance literature:: Multi-step reaction with 2 steps

1: 2.48 g / tetrahydrofuran; hexane / 60 h / 20 °C

2: 86 percent / CuI; Et₃N / PdCl₂(PPh₃)2 / tetrahydrofuran / 0.5 h / 20 °C

With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; hexane;