tert-butyl 1-(2-methoxy-6-pentadecylbenzyl)-6-morpholino-1,4-diazepan-5-one

Base Information

Chemical Name:tert-butyl 1-(2-methoxy-6-pentadecylbenzyl)-6-morpholino-1,4-diazepan-5-one
CAS No.:1363400-76-3
Molecular Formula:C₃₂H₅₅N₃O₃
Molecular Weight:529.807
Hs Code.:

Synonyms:tert-butyl 1-(2-methoxy-6-pentadecylbenzyl)-6-morpholino-1,4-diazepan-5-one

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Chemical Property of tert-butyl 1-(2-methoxy-6-pentadecylbenzyl)-6-morpholino-1,4-diazepan-5-one

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Technology Process of tert-butyl 1-(2-methoxy-6-pentadecylbenzyl)-6-morpholino-1,4-diazepan-5-one

There total 4 articles about tert-butyl 1-(2-methoxy-6-pentadecylbenzyl)-6-morpholino-1,4-diazepan-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.1%

: 1363400-49-0
C₉H₁₇N₃O₂

: 1361955-58-9
methanesulfonic acid 2-methoxy-6-pentadecyl-benzyl ester

: 1363400-76-3
tert-butyl 1-(2-methoxy-6-pentadecylbenzyl)-6-morpholino-1,4-diazepan-5-one

Guidance literature:: With triethylamine; In acetonitrile; at 85 ℃;
DOI:10.2174/157018011796235167

Reference yield:

: 16611-84-0
6-Pentadecylsalicylic Acid

: 1363400-76-3
tert-butyl 1-(2-methoxy-6-pentadecylbenzyl)-6-morpholino-1,4-diazepan-5-one

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetonitrile / 24 h / 90 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 18.67 h / 0 - 20 °C

3: triethylamine / dichloromethane / 3.25 h / 0 - 20 °C

4: triethylamine / acetonitrile / 85 °C

With lithium aluminium tetrahydride; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.2174/157018011796235167

Reference yield:

: 65446-29-9
2-methoxy-6-pentadecyl-benzoic acid methyl ester

: 1363400-76-3
tert-butyl 1-(2-methoxy-6-pentadecylbenzyl)-6-morpholino-1,4-diazepan-5-one

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 18.67 h / 0 - 20 °C

2: triethylamine / dichloromethane / 3.25 h / 0 - 20 °C

3: triethylamine / acetonitrile / 85 °C

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.2174/157018011796235167