2,3,4-Tri-O-acetyl-1-S-benzoyl-5,6-dideoxy-6-C-(2,4-dichlorophenyl)-1-thio-D-xylo-hexitol

Base Information

• Chemical Name: 2,3,4-Tri-O-acetyl-1-S-benzoyl-5,6-dideoxy-6-C-(2,4-dichlorophenyl)-1-thio-D-xylo-hexitol
• CAS No.: 141240-43-9
• Molecular Formula: C₂₅H₂₆Cl₂O₇S
• Molecular Weight: 541.449
• Mol file: 141240-43-9.mol

Synonyms:2,3,4-Tri-O-acetyl-1-S-benzoyl-5,6-dideoxy-6-C-(2,4-dichlorophenyl)-1-thio-D-xylo-hexitol

Chemical Property of 2,3,4-Tri-O-acetyl-1-S-benzoyl-5,6-dideoxy-6-C-(2,4-dichlorophenyl)-1-thio-D-xylo-hexitol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,4-Tri-O-acetyl-1-S-benzoyl-5,6-dideoxy-6-C-(2,4-dichlorophenyl)-1-thio-D-xylo-hexitol

There total 1 articles about 2,3,4-Tri-O-acetyl-1-S-benzoyl-5,6-dideoxy-6-C-(2,4-dichlorophenyl)-1-thio-D-xylo-hexitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

thiobenzoic acid potassium salt (28170-13-0) + 2,3,4-Tri-O-acetyl-5,6-dideoxy-6-C-(2,4-dichlorophenyl)-1-O-methanesulfonyl-D-xylo-hexitol (141240-42-8) → 2,3,4-Tri-O-acetyl-1-S-benzoyl-5,6-dideoxy-6-C-(2,4-dichlorophenyl)-1-thio-D-xylo-hexitol (141240-43-9)

Guidance literature:

In acetone; for 4h; Heating;

DOI:10.1016/S0008-6215(00)90499-3

Reference yield: 73.0%

2,3,4-Tri-O-acetyl-1-S-benzoyl-5,6-dideoxy-6-C-(2,4-dichlorophenyl)-1-thio-D-xylo-hexitol (141240-43-9) → Bis<1,5,6-trideoxy-6-C-(2,4-dichlorophenyl)-D-xylo-hexytol> 1,1'-disulfide (141240-44-0)

Guidance literature:

With sodium methylate; In methanol; for 2h; Ambient temperature;

DOI:10.1016/S0008-6215(00)90499-3

upstream raw materials:

thiobenzoic acid potassium salt

2,3,4-Tri-O-acetyl-5,6-dideoxy-6-C-(2,4-dichlorophenyl)-1-O-methanesulfonyl-D-xylo-hexitol

Downstream raw materials:

Bis<1,5,6-trideoxy-6-C-(2,4-dichlorophenyl)-D-xylo-hexytol> 1,1'-disulfide