3-<6-(benzoylamino)-9H-purin-9-yl>cyclopentaneethanol

Base Information

Chemical Name:3-<6-(benzoylamino)-9H-purin-9-yl>cyclopentaneethanol
CAS No.:145259-75-2
Molecular Formula:C₁₉H₂₁N₅O₂
Molecular Weight:351.408
Hs Code.:

Synonyms:3-<6-(benzoylamino)-9H-purin-9-yl>cyclopentaneethanol

Suppliers and Price of 3-<6-(benzoylamino)-9H-purin-9-yl>cyclopentaneethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-<6-(benzoylamino)-9H-purin-9-yl>cyclopentaneethanol

Chemical Property:

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Technology Process of 3-<6-(benzoylamino)-9H-purin-9-yl>cyclopentaneethanol

There total 9 articles about 3-<6-(benzoylamino)-9H-purin-9-yl>cyclopentaneethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 145259-74-1
methyl cis-3-<6-(dibenzoylamino)-9H-purin-9-yl>cyclopentaneacetate

: 145259-75-2
3-<6-(benzoylamino)-9H-purin-9-yl>cyclopentaneethanol

Guidance literature:: With lithium triethylborohydride; In tetrahydrofuran; for 2h; Ambient temperature;
DOI:10.1002/hlca.19920750620

Reference yield:

: 5724-61-8
2-oxabicyclo[3.2.1]octan-3-one

: 145259-75-2
3-<6-(benzoylamino)-9H-purin-9-yl>cyclopentaneethanol

Guidance literature:: Multi-step reaction with 7 steps

1: 80 percent / Na / Heating

2: 93 percent / Ph₃P, DEAD / tetrahydrofuran / 1 h / Ambient temperature

3: 88 percent / NH₃ / methanol / Ambient temperature

4: 1) Ph₃P, DEAD / multistep reaction; various pyrimidine- and purine derivatives; scope of reaction

5: NH₃ / methanol / 1.5 h / 100 °C

6: 80 percent / pyridine, DMAP / CH₂Cl₂ / 2 h / Ambient temperature

7: 68 percent / lithium triethylborohydride / tetrahydrofuran / 2 h / Ambient temperature

With pyridine; dmap; ammonia; sodium; lithium triethylborohydride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/hlca.19920750620

Reference yield:

: 37435-80-6
methyl cis-3-hydroxycyclopentaneacetate

: 145259-75-2
3-<6-(benzoylamino)-9H-purin-9-yl>cyclopentaneethanol

Guidance literature:: Multi-step reaction with 6 steps

1: 93 percent / Ph₃P, DEAD / tetrahydrofuran / 1 h / Ambient temperature

2: 88 percent / NH₃ / methanol / Ambient temperature

3: 1) Ph₃P, DEAD / multistep reaction; various pyrimidine- and purine derivatives; scope of reaction

4: NH₃ / methanol / 1.5 h / 100 °C

5: 80 percent / pyridine, DMAP / CH₂Cl₂ / 2 h / Ambient temperature

6: 68 percent / lithium triethylborohydride / tetrahydrofuran / 2 h / Ambient temperature

With pyridine; dmap; ammonia; lithium triethylborohydride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/hlca.19920750620