Technology Process of C29H27N4SOCl
There total 11 articles about C29H27N4SOCl which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine; triphenylphosphine;
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide;
In
N,N-dimethyl-formamide;
at 120 ℃;
microwave irradiation;
DOI:10.1021/jm061223o
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 68 percent / K2CO3 / methanol / 0 - 20 °C
2: NaH / benzene / 2.5 h / Heating
3: 524 mg / hydrazine monohydrate; HOAc / ethanol / 4 h / Heating
4: 31 percent / PPh3; Et3N / PdCl2(PPh3)2; CuI / dimethylformamide / 120 °C / microwave irradiation
With
sodium hydride; potassium carbonate; hydrazine hydrate; acetic acid; triethylamine; triphenylphosphine;
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide;
In
methanol; ethanol; N,N-dimethyl-formamide; benzene;
4: Sonogashira coupling;
DOI:10.1021/jm061223o
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 96 percent / Et3N / tetrahydrofuran / 0 °C
2: 68 percent / K2CO3 / methanol / 0 - 20 °C
3: NaH / benzene / 2.5 h / Heating
4: 524 mg / hydrazine monohydrate; HOAc / ethanol / 4 h / Heating
5: 31 percent / PPh3; Et3N / PdCl2(PPh3)2; CuI / dimethylformamide / 120 °C / microwave irradiation
With
sodium hydride; potassium carbonate; hydrazine hydrate; acetic acid; triethylamine; triphenylphosphine;
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide;
In
tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; benzene;
5: Sonogashira coupling;
DOI:10.1021/jm061223o