4-oxo-4-(2,3,5,6-tetramethylphenyl)but-2-enoic Acid

Base Information

Chemical Name:4-oxo-4-(2,3,5,6-tetramethylphenyl)but-2-enoic Acid
CAS No.:22659-83-2
Molecular Formula:C₁₄H₁₆O₃
Molecular Weight:232.279
Hs Code.:2918300090
DSSTox Substance ID:DTXSID20372675
Mol file:22659-83-2.mol

Synonyms:4-oxo-4-(2,3,5,6-tetramethylphenyl)but-2-enoic Acid;22659-83-2;DTXSID20372675;FT-0613511

Suppliers and Price of 4-oxo-4-(2,3,5,6-tetramethylphenyl)but-2-enoic Acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-(2,3,5,6-Tetramethylbenzoyl)-acrylicAcid
10g
$ 175.00

TRC
3-(2,3,5,6-Tetramethylbenzoyl)-acrylicAcid
5g
$ 110.00

American Custom Chemicals Corporation
3-(2,3,5,6-TETRAMETHYLBENZOYL)ACRYLIC ACID 95.00%
5MG
$ 499.31

Total 6 raw suppliers

Chemical Property of 4-oxo-4-(2,3,5,6-tetramethylphenyl)but-2-enoic Acid

Chemical Property:

Vapor Pressure:1.52E-08mmHg at 25°C
Refractive Index:1.554
Boiling Point:440.7°C at 760 mmHg
Flash Point:234.5°C
PSA：54.37000
Density:1.12g/cm³
LogP:2.74370
XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:232.109944368
Heavy Atom Count:17
Complexity:318

Purity/Quality:

99%, ^*data from raw suppliers

3-(2,3,5,6-Tetramethylbenzoyl)-acrylicAcid ^*data from reagent suppliers

Safty Information:

Pictogram(s): R36/37/38:Irritating to eyes, respiratory system and skin.;
Hazard Codes:R36/37/38:Irritating to eyes, respiratory system and skin.;
Statements: R36/37/38:Irritating to eyes, respiratory system and skin.;
Safety Statements: S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.; S36:Wear suitable prot

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1C)C(=O)C=CC(=O)O)C)C

Technology Process of 4-oxo-4-(2,3,5,6-tetramethylphenyl)but-2-enoic Acid

There total 1 articles about 4-oxo-4-(2,3,5,6-tetramethylphenyl)but-2-enoic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-31-6
maleic anhydride

: 95-93-2
1,2,4,5-tetramethylbenzene

: 22659-83-2
(E)-4-(2,3,5,6-tetramethylphenyl)-4-oxo-2-butenoic acid

Guidance literature:: With aluminium trichloride;

Reference yield:

: 22659-83-2
(E)-4-(2,3,5,6-tetramethylphenyl)-4-oxo-2-butenoic acid

: C₁₄H₁₅ClO₂

Guidance literature:: With trichlorophosphate; In tetrahydrofuran;
DOI:10.1016/j.ejmech.2013.01.006

Reference yield:

: 22659-83-2
(E)-4-(2,3,5,6-tetramethylphenyl)-4-oxo-2-butenoic acid

: 1429427-93-9
C₂₂H₂₅NO₄

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / tetrahydrofuran

2: tetrahydrofuran

With trichlorophosphate; In tetrahydrofuran;
DOI:10.1016/j.ejmech.2013.01.006