Technology Process of (2-(phenylselanyl)phenyl)methanamine
There total 3 articles about (2-(phenylselanyl)phenyl)methanamine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 20 ℃;
for 45h;
DOI:10.1039/c3cc39269d
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: hydrazine hydrate; sodium methylate / dimethyl sulfoxide; methanol / 0.08 h / Inert atmosphere
1.2: 12 h / 130 °C / Inert atmosphere
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 45 h / 20 °C
With
lithium aluminium tetrahydride; sodium methylate; hydrazine hydrate;
In
tetrahydrofuran; methanol; dimethyl sulfoxide;
DOI:10.1039/c3cc39269d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: magnesium / diethyl ether / Inert atmosphere
1.2: Reflux; Inert atmosphere
1.3: 5 °C
2.1: hydrazine hydrate; sodium methylate / dimethyl sulfoxide; methanol / 0.08 h / Inert atmosphere
2.2: 12 h / 130 °C / Inert atmosphere
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 45 h / 20 °C
With
lithium aluminium tetrahydride; sodium methylate; hydrazine hydrate; magnesium;
In
tetrahydrofuran; methanol; diethyl ether; dimethyl sulfoxide;
DOI:10.1039/c3cc39269d
