6,7-dimethoxy-2-(4-methoxyphenyl)-1-nitromethyl-1,2,3,4-tetrahydroisoquinoline

Base Information

Chemical Name:6,7-dimethoxy-2-(4-methoxyphenyl)-1-nitromethyl-1,2,3,4-tetrahydroisoquinoline
CAS No.:1132765-78-6
Molecular Formula:C₁₉H₂₂N₂O₅
Molecular Weight:358.394
Hs Code.:

Synonyms:6,7-dimethoxy-2-(4-methoxyphenyl)-1-nitromethyl-1,2,3,4-tetrahydroisoquinoline

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Chemical Property of 6,7-dimethoxy-2-(4-methoxyphenyl)-1-nitromethyl-1,2,3,4-tetrahydroisoquinoline

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Technology Process of 6,7-dimethoxy-2-(4-methoxyphenyl)-1-nitromethyl-1,2,3,4-tetrahydroisoquinoline

There total 2 articles about 6,7-dimethoxy-2-(4-methoxyphenyl)-1-nitromethyl-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 75-52-5
nitromethane

: 1132765-73-1
2-(6,7-dimethoxy-2-(4-methoxyphenyl)-1,2,3,4-tetrahydroisoquinolin-1-yl)acrylaldehyde

: 1132765-78-6
6,7-dimethoxy-2-(4-methoxyphenyl)-1-nitromethyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With 4,4-difluoro-8-phenyl-4-bora-3a,4a-diaza-s-indacene; at 20 ℃; for 3h; Irradiation;
DOI:10.1039/c5cc03421c

Reference yield:

: 696-62-8
para-iodoanisole

: 1132765-78-6
6,7-dimethoxy-2-(4-methoxyphenyl)-1-nitromethyl-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: potassium phosphate; copper(l) iodide; ethylene glycol / isopropyl alcohol / 24 h / 90 °C / Schlenk technique; Inert atmosphere

2: 4,4-difluoro-8-phenyl-4-bora-3a,4a-diaza-s-indacene / 3 h / 20 °C / Irradiation

With 4,4-difluoro-8-phenyl-4-bora-3a,4a-diaza-s-indacene; potassium phosphate; copper(l) iodide; ethylene glycol; In isopropyl alcohol;
DOI:10.1039/c5cc03421c