(2'S,3'S,4'S,5'S,6'R)-7-O-<2'-<3'-iodo-6'-phenyl-4',5'-bis<(trimethylsilyl)oxy>tetrahydropyranosyl>>daunomycinone

Base Information

Chemical Name:(2'S,3'S,4'S,5'S,6'R)-7-O-<2'-<3'-iodo-6'-phenyl-4',5'-bis<(trimethylsilyl)oxy>tetrahydropyranosyl>>daunomycinone
CAS No.:138407-83-7
Molecular Formula:C₃₈H₄₅IO₁₁Si₂
Molecular Weight:860.844
Hs Code.:

Synonyms:(2'S,3'S,4'S,5'S,6'R)-7-O-<2'-<3'-iodo-6'-phenyl-4',5'-bis<(trimethylsilyl)oxy>tetrahydropyranosyl>>daunomycinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2'S,3'S,4'S,5'S,6'R)-7-O-<2'-<3'-iodo-6'-phenyl-4',5'-bis<(trimethylsilyl)oxy>tetrahydropyranosyl>>daunomycinone

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Technology Process of (2'S,3'S,4'S,5'S,6'R)-7-O-<2'-<3'-iodo-6'-phenyl-4',5'-bis<(trimethylsilyl)oxy>tetrahydropyranosyl>>daunomycinone

There total 30 articles about (2'S,3'S,4'S,5'S,6'R)-7-O-<2'-<3'-iodo-6'-phenyl-4',5'-bis<(trimethylsilyl)oxy>tetrahydropyranosyl>>daunomycinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21794-55-8
(+)-Daunomycinone

: 138432-66-3
(-)-(2R,3S,4R)-2-phenyl-3,4-bis<(trimethylsilyl)oxy>-2,3-dihydro-4H-pyran

: 138407-83-7,138512-18-2
(8S,10S)-8-Acetyl-6,8,11-trihydroxy-10-((2R,3R,4S,5S,6R)-3-iodo-6-phenyl-4,5-bis-trimethylsilanyloxy-tetrahydro-pyran-2-yloxy)-1-methoxy-7,8,9,10-tetrahydro-naphthacene-5,12-dione

: 138407-83-7,138512-18-2
(8S,10S)-8-Acetyl-6,8,11-trihydroxy-10-((2S,3R,4S,5S,6R)-3-iodo-6-phenyl-4,5-bis-trimethylsilanyloxy-tetrahydro-pyran-2-yloxy)-1-methoxy-7,8,9,10-tetrahydro-naphthacene-5,12-dione

: 138407-83-7
(2'S,3'S,4'S,5'S,6'R)-7-O-<2'-<3'-iodo-6'-phenyl-4',5'-bis<(trimethylsilyl)oxy>tetrahydropyranosyl>>daunomycinone

Guidance literature:: With 4 A molecular sieve; di-syn-collidinyliodonium perchlorate; In dichloromethane; at 0 ℃; for 1h; Yield given. Title compound not separated from byproducts;

Reference yield:

: 21794-55-8
(+)-Daunomycinone

: 138432-66-3
(-)-(2R,3S,4R)-2-phenyl-3,4-bis<(trimethylsilyl)oxy>-2,3-dihydro-4H-pyran

: 138407-83-7,138512-18-2
(8S,10S)-8-Acetyl-6,8,11-trihydroxy-10-((2R,3R,4S,5S,6R)-3-iodo-6-phenyl-4,5-bis-trimethylsilanyloxy-tetrahydro-pyran-2-yloxy)-1-methoxy-7,8,9,10-tetrahydro-naphthacene-5,12-dione

: 138407-83-7,138512-18-2
(8S,10S)-8-Acetyl-6,8,11-trihydroxy-10-((2S,3R,4S,5S,6R)-3-iodo-6-phenyl-4,5-bis-trimethylsilanyloxy-tetrahydro-pyran-2-yloxy)-1-methoxy-7,8,9,10-tetrahydro-naphthacene-5,12-dione

: 138407-83-7
(2'S,3'S,4'S,5'S,6'R)-7-O-<2'-<3'-iodo-6'-phenyl-4',5'-bis<(trimethylsilyl)oxy>tetrahydropyranosyl>>daunomycinone

Guidance literature:: With 4 A molecular sieve; di-syn-collidinyliodonium perchlorate; In dichloromethane; at 0 ℃; for 1h; Yield given. Title compound not separated from byproducts;

Reference yield:

: 21794-55-8
(+)-Daunomycinone

: 138432-66-3
(-)-(2R,3S,4R)-2-phenyl-3,4-bis<(trimethylsilyl)oxy>-2,3-dihydro-4H-pyran

: 138407-83-7,138512-18-2
(8S,10S)-8-Acetyl-6,8,11-trihydroxy-10-((2R,3R,4S,5S,6R)-3-iodo-6-phenyl-4,5-bis-trimethylsilanyloxy-tetrahydro-pyran-2-yloxy)-1-methoxy-7,8,9,10-tetrahydro-naphthacene-5,12-dione

: 138407-83-7,138512-18-2
(8S,10S)-8-Acetyl-6,8,11-trihydroxy-10-((2S,3R,4S,5S,6R)-3-iodo-6-phenyl-4,5-bis-trimethylsilanyloxy-tetrahydro-pyran-2-yloxy)-1-methoxy-7,8,9,10-tetrahydro-naphthacene-5,12-dione

: 138407-83-7
(2'S,3'S,4'S,5'S,6'R)-7-O-<2'-<3'-iodo-6'-phenyl-4',5'-bis<(trimethylsilyl)oxy>tetrahydropyranosyl>>daunomycinone

Guidance literature:: With 4 A molecular sieve; di-syn-collidinyliodonium perchlorate; In dichloromethane; at 0 ℃; for 1h; Yield given. Title compound not separated from byproducts;