t-Butyl N-(2-{2-Oxo-3-[1-(1-phenylcycloheptyl)-4-piperidinyl]2,3-dihydro-1H-benzimidazol-1-yl}ethyl)carbamate

Base Information

• Chemical Name: t-Butyl N-(2-{2-Oxo-3-[1-(1-phenylcycloheptyl)-4-piperidinyl]2,3-dihydro-1H-benzimidazol-1-yl}ethyl)carbamate
• CAS No.: 231962-50-8
• Molecular Formula: C₃₂H₄₄N₄O₃
• Molecular Weight: 532.726

Synonyms:t-Butyl N-(2-{2-Oxo-3-[1-(1-phenylcycloheptyl)-4-piperidinyl]2,3-dihydro-1H-benzimidazol-1-yl}ethyl)carbamate

Chemical Property of t-Butyl N-(2-{2-Oxo-3-[1-(1-phenylcycloheptyl)-4-piperidinyl]2,3-dihydro-1H-benzimidazol-1-yl}ethyl)carbamate

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Technology Process of t-Butyl N-(2-{2-Oxo-3-[1-(1-phenylcycloheptyl)-4-piperidinyl]2,3-dihydro-1H-benzimidazol-1-yl}ethyl)carbamate

There total 1 articles about t-Butyl N-(2-{2-Oxo-3-[1-(1-phenylcycloheptyl)-4-piperidinyl]2,3-dihydro-1H-benzimidazol-1-yl}ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-[1-(1-phenylcycloheptyl)-4-piperidinyl]-1,3-dihydro-2H-1,3-benzimidazol-2-one (231960-72-8) + 2-(tert-butoxycarbonylamino)ethyl bromide (39684-80-5) → t-Butyl N-(2-{2-Oxo-3-[1-(1-phenylcycloheptyl)-4-piperidinyl]2,3-dihydro-1H-benzimidazol-1-yl}ethyl)carbamate (231962-50-8)

Guidance literature:

With potassium tert-butylate; sodium iodide; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

t-Butyl N-(2-{2-Oxo-3-[1-(1-phenylcycloheptyl)-4-piperidinyl]2,3-dihydro-1H-benzimidazol-1-yl}ethyl)carbamate (231962-50-8) → 1-[2-(Methylamino)ethyl]-3-[1-(1-phenylcycloheptyl)-4-piperidinyl]-1,3-dihydro-2H-benzimidazol-2-one (231961-21-0)

Guidance literature:

With hydrogenchloride; NaH; methyl iodide; In tetrahydrofuran; methanol;

Reference yield:

WSCD-HCl + t-Butyl N-(2-{2-Oxo-3-[1-(1-phenylcycloheptyl)-4-piperidinyl]2,3-dihydro-1H-benzimidazol-1-yl}ethyl)carbamate (231962-50-8) + 1-(tert-butoxycarbonyl)-L-proline (15761-39-4,59433-50-0) → (2R)-N-(2-{2-Oxo-3-[1-(1-phenylcycloheptyl)-4-piperidinyl]-2,3-dihydro-1H-benzimidazol-1-yl}ethyl)tetrahydro-1H-pyrrole-2-carboxamide dihydrochloride

Guidance literature:

With hydrogenchloride; triethylamine; In methanol; N,N-dimethyl-formamide;

upstream raw materials:

1-[1-(1-phenylcycloheptyl)-4-piperidinyl]-1,3-dihydro-2H-1,3-benzimidazol-2-one

2-(tert-butoxycarbonylamino)ethyl bromide

Downstream raw materials:

1-[2-(Methylamino)ethyl]-3-[1-(1-phenylcycloheptyl)-4-piperidinyl]-1,3-dihydro-2H-benzimidazol-2-one

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