tert-butyl 3-[ethoxy({[(2,4,6-triisopropylphenyl)sulfonyl]amino}methyl)phosphoryl]propanoate

Base Information

Chemical Name:tert-butyl 3-[ethoxy({[(2,4,6-triisopropylphenyl)sulfonyl]amino}methyl)phosphoryl]propanoate
CAS No.:1067502-84-4
Molecular Formula:C₂₅H₄₄NO₆PS
Molecular Weight:517.667
Hs Code.:

Synonyms:tert-butyl 3-[ethoxy({[(2,4,6-triisopropylphenyl)sulfonyl]amino}methyl)phosphoryl]propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 3-[ethoxy({[(2,4,6-triisopropylphenyl)sulfonyl]amino}methyl)phosphoryl]propanoate

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Technology Process of tert-butyl 3-[ethoxy({[(2,4,6-triisopropylphenyl)sulfonyl]amino}methyl)phosphoryl]propanoate

There total 1 articles about tert-butyl 3-[ethoxy({[(2,4,6-triisopropylphenyl)sulfonyl]amino}methyl)phosphoryl]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 1067502-49-1
ethyl ({[(2,4,6-triisopropylphenyl)sulfonyl]amino}methyl)phosphinate

: 1067502-84-4
tert-butyl 3-[ethoxy({[(2,4,6-triisopropylphenyl)sulfonyl]amino}methyl)phosphoryl]propanoate

Guidance literature:: With methylmagnesium bromide; tert-butyl alcohol; In tetrahydrofuran; hexane; at 0 ℃; stereospecific reaction;
DOI:10.1021/ol801743d

Reference yield:

: 1067502-84-4
tert-butyl 3-[ethoxy({[(2,4,6-triisopropylphenyl)sulfonyl]amino}methyl)phosphoryl]propanoate

: 100-39-0
benzyl bromide

: tert-butyl (2SR)-2-benzyl-3-[(SR)-ethoxy({[(2,4,6-triisopropylphenyl)sulfonyl]amino}methyl)phosphoryl]propanoate

: tert-butyl (2SR)-2-benzyl-3-[(RS)-ethoxy({[(2,4,6-triisopropylphenyl)sulfonyl]amino}methyl)phosphoryl]propanoate

Guidance literature:: tert-butyl 3-[ethoxy({[(2,4,6-triisopropylphenyl)sulfonyl]amino}methyl)phosphoryl]propanoate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h;

benzyl bromide; In tetrahydrofuran; at -78 ℃; for 2h; optical yield given as %de; diastereoselective reaction;
DOI:10.1021/ol801743d