(+/-)-[2-d1]-4-(tert-butyldimethylsilyloxy)-2-(p-toluenesulfonyloxy)butane

Base Information

Chemical Name:(+/-)-[2-d1]-4-(tert-butyldimethylsilyloxy)-2-(p-toluenesulfonyloxy)butane
CAS No.:1337571-67-1
Molecular Formula:C₁₇H₃₀O₄SSi
Molecular Weight:359.566
Hs Code.:

Synonyms:(+/-)-[2-d1]-4-(tert-butyldimethylsilyloxy)-2-(p-toluenesulfonyloxy)butane

Suppliers and Price of (+/-)-[2-d1]-4-(tert-butyldimethylsilyloxy)-2-(p-toluenesulfonyloxy)butane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-[2-d1]-4-(tert-butyldimethylsilyloxy)-2-(p-toluenesulfonyloxy)butane

Chemical Property:

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Technology Process of (+/-)-[2-d1]-4-(tert-butyldimethylsilyloxy)-2-(p-toluenesulfonyloxy)butane

There total 3 articles about (+/-)-[2-d1]-4-(tert-butyldimethylsilyloxy)-2-(p-toluenesulfonyloxy)butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1337571-66-0
(+/-)-[2-d1]-4-(tert-butyldimethylsilyloxy)-2-butanol

: 98-59-9
p-toluenesulfonyl chloride

: 1337571-67-1
(+/-)-[2-d1]-4-(tert-butyldimethylsilyloxy)-2-(p-toluenesulfonyloxy)butane

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1002/jlcr.1884

Reference yield:

: 120591-36-8
4-(tert-butyldimethylsilyloxy)butan-2-one

: 1337571-67-1
(+/-)-[2-d1]-4-(tert-butyldimethylsilyloxy)-2-(p-toluenesulfonyloxy)butane

Guidance literature:: Multi-step reaction with 2 steps

1: sodium borodeuteride / methanol / 0.25 h

2: pyridine / dichloromethane / 20 h / 20 °C / Inert atmosphere

With pyridine; sodium borodeuteride; In methanol; dichloromethane;
DOI:10.1002/jlcr.1884

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1337571-67-1
(+/-)-[2-d1]-4-(tert-butyldimethylsilyloxy)-2-(p-toluenesulfonyloxy)butane

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / dichloromethane / 1.5 h / Inert atmosphere

2: sodium borodeuteride / methanol / 0.25 h

3: pyridine / dichloromethane / 20 h / 20 °C / Inert atmosphere

With pyridine; 1H-imidazole; sodium borodeuteride; In methanol; dichloromethane;
DOI:10.1002/jlcr.1884