Technology Process of C27H40O5
There total 5 articles about C27H40O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen;
In
ethyl acetate;
at 20 ℃;
for 2.5h;
DOI:10.1016/j.bmcl.2011.12.137
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
2.1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C
3.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere
3.2: 0 - 20 °C / Inert atmosphere
4.1: palladium on activated charcoal; hydrogen / ethyl acetate / 2.5 h / 20 °C
With
palladium on activated charcoal; hydrogen; sodium hydride; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
3.1: Horner-Wadsworth-Emmons type reaction / 3.2: Horner-Wadsworth-Emmons type reaction;
DOI:10.1016/j.bmcl.2011.12.137
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C
2.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere
2.2: 0 - 20 °C / Inert atmosphere
3.1: palladium on activated charcoal; hydrogen / ethyl acetate / 2.5 h / 20 °C
With
palladium on activated charcoal; hydrogen; sodium hydride; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane; ethyl acetate;
2.1: Horner-Wadsworth-Emmons type reaction / 2.2: Horner-Wadsworth-Emmons type reaction;
DOI:10.1016/j.bmcl.2011.12.137
