bis(2-phenylindenyl)hafnium dichloride

Base Information

Chemical Name:bis(2-phenylindenyl)hafnium dichloride
CAS No.:172414-60-7
Molecular Formula:C₃₀H₂₂Cl₂Hf
Molecular Weight:631.901
Hs Code.:

Synonyms:bis(2-phenylindenyl)hafnium dichloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(2-phenylindenyl)hafnium dichloride

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Technology Process of bis(2-phenylindenyl)hafnium dichloride

There total 1 articles about bis(2-phenylindenyl)hafnium dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 4505-48-0
2-phenylindene

: 13499-05-3
hafnium tetrachloride

: 172414-60-7
bis(2-phenylindenyl)hafnium dichloride

Guidance literature:: With nBuLi; In tetrahydrofuran; toluene; (Ar); reaction of 2-phenylindene with nBuLi in THF at -78°C, warming to room temp., removal of the THF, addn. of HfCl4 in toluene; filtration after 24 h, recrystn. (toluene); elem. anal.;
DOI:10.1021/ja971895r

Reference yield: 42.0%

: 172414-60-7
bis(2-phenylindenyl)hafnium dichloride

: 6921-34-2
benzylmagnesium chloride

: 197955-27-4
bis(2-phenylindenyl)hafnium dibenzyl

Guidance literature:: In tetrahydrofuran; toluene; (Ar); reaction at room temp. for 24 h,removal of the THF, addn. of toluene; recrystn. (toluene; elem. anal.;
DOI:10.1021/ja971895r