Technology Process of {R,R-1,2-bis((phenyl-o-anisoyl)phosphino)ethane}rhodium(I) tetrafluoroborate
There total 1 articles about {R,R-1,2-bis((phenyl-o-anisoyl)phosphino)ethane}rhodium(I) tetrafluoroborate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
In
methanol;
stirred under H2 at room temp. until gas uptake ceased (ca 15 min); soln. cooled to -80°C, evacuated, diluted with diethyl ether, after warming to room temp. pptn., filtered in inert atmosphere, precipitate washed with diethyl ether, dried in vac.;
DOI:10.1021/ja00240a025