C₅₇H₆₈O₁₃S

Base Information

Chemical Name:C₅₇H₆₈O₁₃S
CAS No.:925932-33-8
Molecular Formula:C₅₇H₆₈O₁₃S
Molecular Weight:993.225
Hs Code.:

C<sub>57</sub>H<sub>68</sub>O<sub>13</sub>S

Synonyms:C₅₇H₆₈O₁₃S

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Chemical Property of C₅₇H₆₈O₁₃S

Chemical Property:

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Technology Process of C₅₇H₆₈O₁₃S

There total 13 articles about C₅₇H₆₈O₁₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 925932-32-7
C₅₀H₆₂O₁₁

: 98-59-9
p-toluenesulfonyl chloride

: 925932-33-8
C₅₇H₆₈O₁₃S

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.3987/com-06-s(o)44

Reference yield:

: 53380-10-2
1,3-bis((2,2-dimethyl-1,3-dioxolan-4-yl)methoxy)propan-2-ol

: 925932-33-8
C₅₇H₆₈O₁₃S

Guidance literature:: Multi-step reaction with 13 steps

1.1: 93 percent / NaH / tetrahydrofuran

2.1: 100 percent / aq. AcOH

3.1: 95 percent / DMAP; Et₃N / CH₂Cl₂

4.1: NaH / tetrahydrofuran

4.2: 80 percent / tetrabutylammonium fluoride / tetrahydrofuran

5.1: 50 percent / Et₃N / CH₂Cl₂

6.1: NaH / tetrahydrofuran; dimethylsulfoxide

7.1: aq. AcOH

8.1: TBDPSCl; DMAP; Et₃N / CH₂Cl₂

8.2: NaH / tetrahydrofuran

8.3: tetrabutylammonium fluoride / tetrahydrofuran

9.1: 59 percent / Et₃N / CH₂Cl₂

10.1: NaH; DMSO / tetrahydrofuran

11.1: aq. AcOH

12.1: TBDPS-Cl; DMAP; Et₃N / CH₂Cl₂

12.2: NaH / tetrahydrofuran

12.3: tetrabutylammonium fluoride / tetrahydrofuran

13.1: 29 percent / Et₃N / CH₂Cl₂

With dmap; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; tert-butylchlorodiphenylsilane; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide;
DOI:10.3987/com-06-s(o)44

Reference yield:

: 196497-38-8
6-(benzyloxy)-4,8-dioxaundecane-1,2,10,11-tetraol

: 925932-33-8
C₅₇H₆₈O₁₃S

Guidance literature:: Multi-step reaction with 11 steps

1.1: 95 percent / DMAP; Et₃N / CH₂Cl₂

2.1: NaH / tetrahydrofuran

2.2: 80 percent / tetrabutylammonium fluoride / tetrahydrofuran

3.1: 50 percent / Et₃N / CH₂Cl₂

4.1: NaH / tetrahydrofuran; dimethylsulfoxide

5.1: aq. AcOH

6.1: TBDPSCl; DMAP; Et₃N / CH₂Cl₂

6.2: NaH / tetrahydrofuran

6.3: tetrabutylammonium fluoride / tetrahydrofuran

7.1: 59 percent / Et₃N / CH₂Cl₂

8.1: NaH; DMSO / tetrahydrofuran

9.1: aq. AcOH

10.1: TBDPS-Cl; DMAP; Et₃N / CH₂Cl₂

10.2: NaH / tetrahydrofuran

10.3: tetrabutylammonium fluoride / tetrahydrofuran

11.1: 29 percent / Et₃N / CH₂Cl₂

With dmap; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; tert-butylchlorodiphenylsilane; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide;
DOI:10.3987/com-06-s(o)44