(4-benzothiazol-2-yl-phenyl)-[2-(4,6-dichloro-[1,3,5]triazin-2-yloxy)-ethyl]-methyl-amine

Base Information

• Chemical Name: (4-benzothiazol-2-yl-phenyl)-[2-(4,6-dichloro-[1,3,5]triazin-2-yloxy)-ethyl]-methyl-amine
• CAS No.: 958859-18-2
• Molecular Formula: C₁₉H₁₅Cl₂N₅OS
• Molecular Weight: 432.333

Synonyms:(4-benzothiazol-2-yl-phenyl)-[2-(4,6-dichloro-[1,3,5]triazin-2-yloxy)-ethyl]-methyl-amine

Chemical Property of (4-benzothiazol-2-yl-phenyl)-[2-(4,6-dichloro-[1,3,5]triazin-2-yloxy)-ethyl]-methyl-amine

Chemical Property:

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Technology Process of (4-benzothiazol-2-yl-phenyl)-[2-(4,6-dichloro-[1,3,5]triazin-2-yloxy)-ethyl]-methyl-amine

There total 1 articles about (4-benzothiazol-2-yl-phenyl)-[2-(4,6-dichloro-[1,3,5]triazin-2-yloxy)-ethyl]-methyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3,5-trichloro-2,4,6-triazine (108-77-0) + 2-[N-methyl-N-(2-hydroxyethyl)-4-aminophenyl]benzothiazole (958859-11-5) → (4-benzothiazol-2-yl-phenyl)-[2-(4,6-dichloro-[1,3,5]triazin-2-yloxy)-ethyl]-methyl-amine (958859-18-2)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 8h;

DOI:10.1002/anie.200702399

Reference yield:

C6H5PolS + (4-benzothiazol-2-yl-phenyl)-[2-(4,6-dichloro-[1,3,5]triazin-2-yloxy)-ethyl]-methyl-amine (958859-18-2) → C25H19ClN5OPolS2

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 65 ℃; Polystyrene

Reference yield:

(4-benzothiazol-2-yl-phenyl)-[2-(4,6-dichloro-[1,3,5]triazin-2-yloxy)-ethyl]-methyl-amine (958859-18-2) + 1,4,7-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane (175854-39-4) → 10-(4-{2-[(4-benzothiazol-2-yl-phenyl)methylamino]ethoxy}-6-chloro-[1,3,5]triazin-2-yl)-1,4,7,10-tetraazacyclododecane-1,4,7-tricarboxylic acid tri-tert-butyl ester (1266708-40-0)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 6h;

DOI:10.1007/s00775-010-0750-y

upstream raw materials:

1,3,5-trichloro-2,4,6-triazine

2-[N-methyl-N-(2-hydroxyethyl)-4-aminophenyl]benzothiazole

Downstream raw materials:

10-(3-{3-[4-{2-[(4-benzothiazol-2-yl-phenyl)-methyl-amino]-ethoxy}-6-(2-methyl-benzylamino)-[1,3,5]triazin-2-ylamino]-propionylamino}-propyl)-1,4,7,10-tetraaza-cyclododecane-1,4,7-tricarboxylic acid tri-tert-butyl ester

10-(3-{2-[4-{2-[(4-benzothiazol-2-yl-phenyl)-methyl-amino]-ethoxy}-6-(4-chloro-benzylamino)-[1,3,5]triazin-2-ylamino]-(S)-propionylamino}-propyl)-1,4,7,10-tetraazacyclododecane-1,4,7-tricarboxylic acid tri-tert-butyl ester

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