Technology Process of C27H23N3O7S2
There total 7 articles about C27H23N3O7S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C10H7N3OS; C23H31FO6SSi;
With
pyridine;
In
tetrahydrofuran;
at 20 ℃;
for 72h;
With
trifluoroacetic acid;
In
methanol; water;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 3.75 h / 0 - 20 °C
2.1: lithium hydroxide; water / tetrahydrofuran; methanol / 3 h / 20 °C
2.2: pH 4
3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 72 h / 20 °C
4.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C
5.1: pyridine; trifluoro-[1,3,5]triazine / dichloromethane / 2 h / -10 - 20 °C
6.1: pyridine / tetrahydrofuran / 72 h / 20 °C
With
pyridine; 1H-imidazole; lithium hydroxide; trifluoro-[1,3,5]triazine; di-isopropyl azodicarboxylate; water; hydrogen; triphenylphosphine;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 72 h / 20 °C
2: 1H-imidazole / N,N-dimethyl-formamide / 20 °C
3: pyridine; trifluoro-[1,3,5]triazine / dichloromethane / 2 h / -10 - 20 °C
4: pyridine / tetrahydrofuran / 72 h / 20 °C
With
pyridine; 1H-imidazole; trifluoro-[1,3,5]triazine; hydrogen;
palladium 10% on activated carbon;
In
tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;