Technology Process of C13H10FN3
There total 7 articles about C13H10FN3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C8H6F3NO4S; 4-fluorophenyhydrazine hydrochloride;
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 3h;
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
N,N-dimethyl-formamide; toluene;
at 100 ℃;
- Guidance literature:
-
With
potassium carbonate;
copper(l) iodide; cis-N,N'-dimethyl-1,2-diaminocyclohexane;
In
N,N-dimethyl-formamide;
at 130 ℃;
for 1h;
microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 2 h
2: acetic anhydride; potassium acetate; acetic acid; isopentyl nitrite / toluene / 2 h / Reflux
3: potassium carbonate; methanol / 0.08 h / Reflux
4: potassium carbonate / cis-N,N'-dimethyl-1,2-diaminocyclohexane; copper(l) iodide / N,N-dimethyl-formamide / 1 h / 130 °C / microwave irradiation
With
methanol; potassium acetate; acetic anhydride; potassium carbonate; acetic acid; triethylamine; isopentyl nitrite;
copper(l) iodide; cis-N,N'-dimethyl-1,2-diaminocyclohexane;
In
dichloromethane; N,N-dimethyl-formamide; toluene;