5-[2-amino-6-(3-carboxypropylsulfanyl)pyrimidin-4-yl]-2,4-dimethylbenzoic acid tert-butyl ester

Base Information

Chemical Name:5-[2-amino-6-(3-carboxypropylsulfanyl)pyrimidin-4-yl]-2,4-dimethylbenzoic acid tert-butyl ester
CAS No.:1052647-55-8
Molecular Formula:C₂₁H₂₇N₃O₄S
Molecular Weight:417.529
Hs Code.:

Synonyms:5-[2-amino-6-(3-carboxypropylsulfanyl)pyrimidin-4-yl]-2,4-dimethylbenzoic acid tert-butyl ester

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Chemical Property of 5-[2-amino-6-(3-carboxypropylsulfanyl)pyrimidin-4-yl]-2,4-dimethylbenzoic acid tert-butyl ester

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Technology Process of 5-[2-amino-6-(3-carboxypropylsulfanyl)pyrimidin-4-yl]-2,4-dimethylbenzoic acid tert-butyl ester

There total 1 articles about 5-[2-amino-6-(3-carboxypropylsulfanyl)pyrimidin-4-yl]-2,4-dimethylbenzoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2906-60-7
5,6-dithia-decanedioic acid

: 1052647-13-8
5-(2-amino-6-chloro-pyrimidin-4-yl)-2,4-dimethylbenzoic acid tert-butyl ester

: 1052647-55-8
5-[2-amino-6-(3-carboxypropylsulfanyl)pyrimidin-4-yl]-2,4-dimethylbenzoic acid tert-butyl ester

Guidance literature:: 5,6-dithia-decanedioic acid; With tributylphosphine; In N,N-dimethyl-formamide; at 20 - 25 ℃; for 1.5h;

5-(2-amino-6-chloro-pyrimidin-4-yl)-2,4-dimethylbenzoic acid tert-butyl ester; With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 2h;

Reference yield:

: 68076-36-8
1-amino-4-[(tert-butyloxycarbonyl)amino]butane

: 1052647-55-8
5-[2-amino-6-(3-carboxypropylsulfanyl)pyrimidin-4-yl]-2,4-dimethylbenzoic acid tert-butyl ester

: 1052647-60-5
5-{2-amino-6-[3-(4-tert-butoxycarbonylaminobutylcarbamoyl)propylsulfanyl]pyrimidin-4-yl}-2, 4-dimethylbenzoic acid tert-butyl ester

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 - 25 ℃; for 2h;

Reference yield:

: 57260-73-8
N-BOC-1,2-diaminoethane

: 1052647-55-8
5-[2-amino-6-(3-carboxypropylsulfanyl)pyrimidin-4-yl]-2,4-dimethylbenzoic acid tert-butyl ester

: 1052647-56-9
5-{2-amino-6-[3-(2-tert-butoxycarbonylaminoethylcarbamoyl)propylsulfanyl]pyrimidin-4-yl}-2, 4-dimethylbenzoic acid tert-butyl ester

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 - 25 ℃; for 12h;