(1S,2S)-threo-2-benzamido-1-(4-methylthiophenyl)-1,3-propanediol

Base Information

Chemical Name:(1S,2S)-threo-2-benzamido-1-(4-methylthiophenyl)-1,3-propanediol
CAS No.:95448-24-1
Molecular Formula:C₁₇H₁₉NO₃S
Molecular Weight:317.409
Hs Code.:

Synonyms:(1S,2S)-threo-2-benzamido-1-(4-methylthiophenyl)-1,3-propanediol

Suppliers and Price of (1S,2S)-threo-2-benzamido-1-(4-methylthiophenyl)-1,3-propanediol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1S,2S)-threo-2-benzamido-1-(4-methylthiophenyl)-1,3-propanediol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1S,2S)-threo-2-benzamido-1-(4-methylthiophenyl)-1,3-propanediol

There total 1 articles about (1S,2S)-threo-2-benzamido-1-(4-methylthiophenyl)-1,3-propanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16854-32-3
(1S,2S)-(+)-thiomicamine

: 98-88-4
benzoyl chloride

: 95448-24-1
(1S,2S)-threo-2-benzamido-1-(4-methylthiophenyl)-1,3-propanediol

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)80813-8

Reference yield: 70.0%

: 95448-24-1
(1S,2S)-threo-2-benzamido-1-(4-methylthiophenyl)-1,3-propanediol

: 95448-25-2
α-Benzoylamino-4-methylthioacetophenone

Guidance literature:: With benzophenone; potassium tert-butylate; In benzene; for 2h; Heating;
DOI:10.1055/s-1984-30988

Reference yield:

: 95448-24-1
(1S,2S)-threo-2-benzamido-1-(4-methylthiophenyl)-1,3-propanediol

: 14172-52-2,16854-32-3,23150-35-8,27348-36-3,27348-47-6,27348-48-7,36624-58-5
2-Amino-1-(4-methylsulfanyl-phenyl)-propane-1,3-diol

Guidance literature:: Multi-step reaction with 5 steps

1: tosyl cloride / CH₂Cl₂ / 40 °C

2: 90 percent / dimethyl sulphoxyde, oxalyl chloride, triethylamine / CH₂Cl₂ / -20 °C

3: 90 percent / sodium borohydride / methanol / -20 °C

4: 1NHCl / 20 °C

5: 10percent w/v NaOH / 100 °C

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; oxalyl dichloride; dimethyl sulfoxide; triethylamine; p-toluenesulfonyl chloride; In methanol; dichloromethane;
DOI:10.1016/S0040-4039(00)80813-8