C₂₃H₃₉N₃O₄Si

Base Information

Chemical Name:C₂₃H₃₉N₃O₄Si
CAS No.:1408058-30-9
Molecular Formula:C₂₃H₃₉N₃O₄Si
Molecular Weight:449.666
Hs Code.:

C<sub>23</sub>H<sub>39</sub>N<sub>3</sub>O<sub>4</sub>Si

Synonyms:C₂₃H₃₉N₃O₄Si

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Chemical Property of C₂₃H₃₉N₃O₄Si

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Technology Process of C₂₃H₃₉N₃O₄Si

There total 12 articles about C₂₃H₃₉N₃O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₃₉F₃O₇SSi

: 1408058-30-9
C₂₃H₃₉N₃O₄Si

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:org/10.1016/j.tetlet.2012.08.143

Reference yield:

: 3458-28-4
D-Mannose

: 1408058-30-9
C₂₃H₃₉N₃O₄Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: sulfuric acid / N,N-dimethyl-formamide / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide

2.2: 4 h / 20 °C

3.1: hydrogenchloride; water / methanol / 4 h / 20 °C

4.1: sodium periodate / ethanol; water; methanol / 3 h / 20 °C

5.1: copper(II) bis(trifluoromethanesulfonate); borane-THF / 2 h / 20 °C / Inert atmosphere

6.1: pyridine / dichloromethane / 2 h / 20 °C

7.1: copper(II) bis(trifluoromethanesulfonate); borane-THF / 0.17 h / 20 °C / Inert atmosphere

8.1: 1H-imidazole; dmap / dichloromethane / 24 h / 20 °C / Inert atmosphere

9.1: pyridine / dichloromethane / 1 h / -15 °C / Inert atmosphere

10.1: sodium azide / N,N-dimethyl-formamide / 2 h / 20 °C

With pyridine; 1H-imidazole; hydrogenchloride; dmap; sodium periodate; sodium azide; borane-THF; sulfuric acid; water; copper(II) bis(trifluoromethanesulfonate); sodium hydride; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:org/10.1016/j.tetlet.2012.08.143

Reference yield:

: 1393086-00-4
C₁₇H₂₂O₅

: 1408058-30-9
C₂₃H₃₉N₃O₄Si

Guidance literature:: Multi-step reaction with 4 steps

1: copper(II) bis(trifluoromethanesulfonate); borane-THF / 2 h / 20 °C / Inert atmosphere

2: 1H-imidazole; dmap / dichloromethane / 24 h / 20 °C / Inert atmosphere

3: pyridine / dichloromethane / 1 h / -15 °C / Inert atmosphere

4: sodium azide / N,N-dimethyl-formamide / 2 h / 20 °C

With pyridine; 1H-imidazole; dmap; sodium azide; borane-THF; copper(II) bis(trifluoromethanesulfonate); In dichloromethane; N,N-dimethyl-formamide;
DOI:org/10.1016/j.tetlet.2012.08.143