allyl 3-(2-allyloxycarbonylmethyl-2-hydroxy-3,3-dimethylcyclohexyl)propanoate

Base Information

Chemical Name:allyl 3-(2-allyloxycarbonylmethyl-2-hydroxy-3,3-dimethylcyclohexyl)propanoate
CAS No.:405200-93-3
Molecular Formula:C₁₉H₃₀O₅
Molecular Weight:338.444
Hs Code.:

Synonyms:allyl 3-(2-allyloxycarbonylmethyl-2-hydroxy-3,3-dimethylcyclohexyl)propanoate

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Chemical Property of allyl 3-(2-allyloxycarbonylmethyl-2-hydroxy-3,3-dimethylcyclohexyl)propanoate

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Technology Process of allyl 3-(2-allyloxycarbonylmethyl-2-hydroxy-3,3-dimethylcyclohexyl)propanoate

There total 4 articles about allyl 3-(2-allyloxycarbonylmethyl-2-hydroxy-3,3-dimethylcyclohexyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 591-87-7
Allyl acetate

: 405200-91-1
allyl 3-(3,3-dimethyl-2-oxocyclohexyl)propanoate

: 405200-93-3
allyl 3-(2-allyloxycarbonylmethyl-2-hydroxy-3,3-dimethylcyclohexyl)propanoate

Guidance literature:: Allyl acetate; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -70 ℃; for 0.5h;

allyl 3-(3,3-dimethyl-2-oxocyclohexyl)propanoate; In tetrahydrofuran; hexane; at -70 ℃; for 2h;
DOI:10.1039/b104394n

Reference yield:

: 67978-74-9
3-(3,3-Dimethyl-2-oxo-cyclohexyl)-propionic acid

: 405200-93-3
allyl 3-(2-allyloxycarbonylmethyl-2-hydroxy-3,3-dimethylcyclohexyl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 4.79 g / DCC; DMAP / CH₂Cl₂ / 2 h / 20 °C

2.1: LDA / tetrahydrofuran; hexane / 0.5 h / -70 °C

2.2: 82 percent / tetrahydrofuran; hexane / 2 h / -70 °C

With dmap; dicyclohexyl-carbodiimide; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1039/b104394n

Reference yield:

: 101327-97-3
Methyl 3,3-dimethyl-2-oxocyclohexanecarboxylate

: 405200-93-3
allyl 3-(2-allyloxycarbonylmethyl-2-hydroxy-3,3-dimethylcyclohexyl)propanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaOEt / benzene / 6 h / 0 °C

2.1: aq. HCl / 18 h / Heating

3.1: 4.79 g / DCC; DMAP / CH₂Cl₂ / 2 h / 20 °C

4.1: LDA / tetrahydrofuran; hexane / 0.5 h / -70 °C

4.2: 82 percent / tetrahydrofuran; hexane / 2 h / -70 °C

With hydrogenchloride; dmap; sodium ethanolate; dicyclohexyl-carbodiimide; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; benzene;
DOI:10.1039/b104394n