4-(menthyloxyacetoxybenzoyloxy)biphenyl-4'-(2-(undec-10-enoyloxyhexyloxy))benzoate

Base Information

• Chemical Name: 4-(menthyloxyacetoxybenzoyloxy)biphenyl-4'-(2-(undec-10-enoyloxyhexyloxy))benzoate
• CAS No.: 1422559-79-2
• Molecular Formula: C₅₅H₆₈O₁₀
• Molecular Weight: 889.139
• Mol file: 1422559-79-2.mol

Synonyms:4-(menthyloxyacetoxybenzoyloxy)biphenyl-4'-(2-(undec-10-enoyloxyhexyloxy))benzoate

Chemical Property of 4-(menthyloxyacetoxybenzoyloxy)biphenyl-4'-(2-(undec-10-enoyloxyhexyloxy))benzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(menthyloxyacetoxybenzoyloxy)biphenyl-4'-(2-(undec-10-enoyloxyhexyloxy))benzoate

There total 10 articles about 4-(menthyloxyacetoxybenzoyloxy)biphenyl-4'-(2-(undec-10-enoyloxyhexyloxy))benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

4-hydroxybiphenyl-4'-(6-undec-10-enoyloxyhexyloxy)benzoate (1384159-16-3) + C19H25ClO4 (1189123-66-7) → 4-(menthyloxyacetoxybenzoyloxy)biphenyl-4'-(2-(undec-10-enoyloxyhexyloxy))benzoate (1422559-79-2)

Guidance literature:

With pyridine; In chloroform; at 20 ℃; for 26h; Reflux;

DOI:10.1002/pola.26350

Reference yield:

1,6-hexanediol (629-11-8) → 4-(menthyloxyacetoxybenzoyloxy)biphenyl-4'-(2-(undec-10-enoyloxyhexyloxy))benzoate (1422559-79-2)

Guidance literature:

Multi-step reaction with 5 steps

1: potassium hydroxide; potassium iodide

2: N,N-dimethyl-formamide; tetrahydrofuran

3: thionyl chloride / N,N-dimethyl-formamide

4: pyridine / tetrahydrofuran / 14 h / 20 - 65 °C

5: pyridine / chloroform / 26 h / 20 °C / Reflux

With pyridine; thionyl chloride; potassium iodide; potassium hydroxide; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;

DOI:10.1002/pola.26350

Reference yield:

6-chloro-1-hexanol (2009-83-8) → 4-(menthyloxyacetoxybenzoyloxy)biphenyl-4'-(2-(undec-10-enoyloxyhexyloxy))benzoate (1422559-79-2)

Guidance literature:

Multi-step reaction with 6 steps

1: water / ethanol

2: potassium hydroxide; potassium iodide

3: N,N-dimethyl-formamide; tetrahydrofuran

4: thionyl chloride / N,N-dimethyl-formamide

5: pyridine / tetrahydrofuran / 14 h / 20 - 65 °C

6: pyridine / chloroform / 26 h / 20 °C / Reflux

With pyridine; thionyl chloride; water; potassium iodide; potassium hydroxide; In tetrahydrofuran; ethanol; chloroform; N,N-dimethyl-formamide;

DOI:10.1002/pola.26350

upstream raw materials:

4-hydroxybiphenyl-4'-(6-undec-10-enoyloxyhexyloxy)benzoate

C₁₉H₂₅ClO₄

(-)-menthol

6-chloro-1-hexanol