C₂₄H₃₅N₃O₄*C₂HF₃O₂

Base Information

Chemical Name:C₂₄H₃₅N₃O₄*C₂HF₃O₂
CAS No.:1446712-17-9
Molecular Formula:C₂HF₃O₂*C₂₄H₃₅N₃O₄
Molecular Weight:543.584
Hs Code.:

C<sub>24</sub>H<sub>35</sub>N<sub>3</sub>O<sub>4</sub>*C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>

Synonyms:C₂₄H₃₅N₃O₄*C₂HF₃O₂

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Chemical Property of C₂₄H₃₅N₃O₄*C₂HF₃O₂

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Technology Process of C₂₄H₃₅N₃O₄*C₂HF₃O₂

There total 16 articles about C₂₄H₃₅N₃O₄*C₂HF₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1431768-60-3
C₃₂H₄₁N₃O₆

: 1446712-17-9
C₂₄H₃₅N₃O₄*C₂HF₃O₂

Guidance literature:: With palladium on activated charcoal; hydrogen; trifluoroacetic acid; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1021/jm4002296

Reference yield:

: C₄₅H₄₉NO₃Si

: 1446712-17-9
C₂₄H₃₅N₃O₄*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 10 steps

1: hydrogenchloride / ethyl acetate; water; methanol / 2 h / 20 °C

2: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

3: sodium chlorite; sodium dihydrogen phosphate dihydrate; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol / 5 h / 20 °C

4: triethylamine; diphenyl phosphoryl azide / dichloromethane / 15.33 h / 0 - 20 °C

5: 17 h / Reflux

6: potassium carbonate; methanol / 23 h / 20 °C

7: triethylamine / dichloromethane / 17 h / 0 - 20 °C

8: trifluoroacetic acid / dichloromethane / 0.17 h / 20 °C

9: triethylamine / dichloromethane / 20 h / 0 - 20 °C

10: trifluoroacetic acid; hydrogen; palladium on activated charcoal / dichloromethane / 2 h / 0 °C

With hydrogenchloride; methanol; sodium chlorite; 2-methyl-but-2-ene; sodium dihydrogen phosphate dihydrate; diphenyl phosphoryl azide; palladium on activated charcoal; hydrogen; potassium carbonate; Dess-Martin periodane; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol;
DOI:10.1021/jm4002296

Reference yield:

: C₃₀H₃₉NOSi

: 1446712-17-9
C₂₄H₃₅N₃O₄*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 11 steps

1: sodium carbonate / tetrahydrofuran; water / 36 h / 20 °C

2: hydrogenchloride / ethyl acetate; water; methanol / 2 h / 20 °C

3: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

4: sodium chlorite; sodium dihydrogen phosphate dihydrate; 2-methyl-but-2-ene / tetrahydrofuran; water; tert-butyl alcohol / 5 h / 20 °C

5: triethylamine; diphenyl phosphoryl azide / dichloromethane / 15.33 h / 0 - 20 °C

6: 17 h / Reflux

7: potassium carbonate; methanol / 23 h / 20 °C

8: triethylamine / dichloromethane / 17 h / 0 - 20 °C

9: trifluoroacetic acid / dichloromethane / 0.17 h / 20 °C

10: triethylamine / dichloromethane / 20 h / 0 - 20 °C

11: trifluoroacetic acid; hydrogen; palladium on activated charcoal / dichloromethane / 2 h / 0 °C

With hydrogenchloride; methanol; sodium chlorite; 2-methyl-but-2-ene; sodium dihydrogen phosphate dihydrate; diphenyl phosphoryl azide; palladium on activated charcoal; hydrogen; sodium carbonate; potassium carbonate; Dess-Martin periodane; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol;
DOI:10.1021/jm4002296