Benzyl-α-d Nitrate

Base Information

• Chemical Name: Benzyl-α-d Nitrate
• CAS No.: 76946-77-5
• Molecular Formula: C₇H₇NO₃
• Molecular Weight: 154.13
• Mol file: 76946-77-5.mol

Synonyms:Benzyl-α-d Nitrate

Chemical Property of Benzyl-α-d Nitrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzyl-α-d Nitrate

There total 3 articles about Benzyl-α-d Nitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(chloromethyl-d)benzene (79449-94-8) → Benzyl-α-d Nitrate (76946-77-5)

Guidance literature:

With silver nitrate; In acetonitrile; for 120h; Yield given; Ambient temperature;

DOI:10.1021/jo00342a017

Reference yield:

benzaldehyde (100-52-7) → Benzyl-α-d Nitrate (76946-77-5)

Guidance literature:

Multistep reaction;

DOI:10.1021/jo00322a062

Reference yield:

benzyl alcohol-d1 (3481-15-0,4181-90-2,52949-66-3,4546-45-6) → Benzyl-α-d Nitrate (76946-77-5)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂, pyridine / 2 h / Heating

2: AgNO₃ / acetonitrile / Ambient temperature

With pyridine; thionyl chloride; silver nitrate; In acetonitrile;

DOI:10.1021/jo00338a015

upstream raw materials:

(chloromethyl-d)benzene

benzaldehyde

benzyl alcohol-d1

Downstream raw materials:

Benzaldehyde-d

benzaldehyde