4-(5,6-dichloro-2-benzimidazolyl)-3-phenylbutanoic acid hydrochloride

Base Information

Chemical Name:4-(5,6-dichloro-2-benzimidazolyl)-3-phenylbutanoic acid hydrochloride
CAS No.:1221962-09-9
Molecular Formula:C₁₇H₁₄Cl₂N₂O₂*ClH
Molecular Weight:385.677
Hs Code.:

Synonyms:4-(5,6-dichloro-2-benzimidazolyl)-3-phenylbutanoic acid hydrochloride

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Chemical Property of 4-(5,6-dichloro-2-benzimidazolyl)-3-phenylbutanoic acid hydrochloride

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Technology Process of 4-(5,6-dichloro-2-benzimidazolyl)-3-phenylbutanoic acid hydrochloride

There total 4 articles about 4-(5,6-dichloro-2-benzimidazolyl)-3-phenylbutanoic acid hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4160-80-9
3-phenylglutaric acid anhydride

: 1221962-09-9
4-(5,6-dichloro-2-benzimidazolyl)-3-phenylbutanoic acid hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 0.5 h / 20 °C

1.2: Reflux

2.1: hydrogenchloride; acetic acid / water / 20 °C / Reflux

With hydrogenchloride; acetic acid; In tetrahydrofuran; water;

Reference yield:

: 1221962-08-8
7,8-dichloro-3-phenyl-3,4-dihydropyrido[1,2-a]benzimidazol-1(2H)-one

: 1221962-09-9
4-(5,6-dichloro-2-benzimidazolyl)-3-phenylbutanoic acid hydrochloride

Guidance literature:: With hydrogenchloride; acetic acid; In water; at 20 ℃; Reflux;

Reference yield:

: 100-52-7
benzaldehyde

: 1221962-09-9
4-(5,6-dichloro-2-benzimidazolyl)-3-phenylbutanoic acid hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: piperidine / 72 h / 20 °C / Cooling with ice

1.2: 2 h / Reflux

2.1: acetyl chloride / 2 h / Reflux

3.1: tetrahydrofuran / 0.5 h / 20 °C

3.2: Reflux

4.1: hydrogenchloride; acetic acid / water / 20 °C / Reflux

With piperidine; hydrogenchloride; acetic acid; acetyl chloride; In tetrahydrofuran; water;