2,6-bis(6-((4-nitrophenoxy)methyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl)pyridine

Base Information

Chemical Name:2,6-bis(6-((4-nitrophenoxy)methyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl)pyridine
CAS No.:1620888-42-7
Molecular Formula:C₂₅H₁₅N₁₁O₆S₂
Molecular Weight:629.596
Hs Code.:

Synonyms:2,6-bis(6-((4-nitrophenoxy)methyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl)pyridine

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Chemical Property of 2,6-bis(6-((4-nitrophenoxy)methyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl)pyridine

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Technology Process of 2,6-bis(6-((4-nitrophenoxy)methyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl)pyridine

There total 5 articles about 2,6-bis(6-((4-nitrophenoxy)methyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1798-11-4
4-nitrophenoxyacetic acid

: 944727-77-9
5,5'-(pyridine-2,6-diyl)bis(4-amino-3-mercapto-1,2,4-triazole)

: 1620888-42-7
2,6-bis(6-((4-nitrophenoxy)methyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl)pyridine

Guidance literature:: With trichlorophosphate; at 106 ℃; for 7h;
DOI:10.1016/j.molstruc.2014.06.026

Reference yield:

: 499-83-2
Pyridine-2,6-dicarboxylic acid

: 1620888-42-7
2,6-bis(6-((4-nitrophenoxy)methyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl)pyridine

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetyl chloride

2.1: hydrazine / ethanol / 6 h / 85 °C / Reflux

3.1: potassium hydroxide; carbon disulfide / ethanol / 14 h / 20 °C

3.2: 6 h / 110 °C

4.1: trichlorophosphate / 7 h / 106 °C

With carbon disulfide; acetyl chloride; potassium hydroxide; hydrazine; trichlorophosphate; In ethanol;
DOI:10.1016/j.molstruc.2014.06.026

Reference yield:

: 5112-36-7
pyridine-2,6-dicarbohydrazide

: 1620888-42-7
2,6-bis(6-((4-nitrophenoxy)methyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl)pyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide; carbon disulfide / ethanol / 14 h / 20 °C

1.2: 6 h / 110 °C

2.1: trichlorophosphate / 7 h / 106 °C

With carbon disulfide; potassium hydroxide; trichlorophosphate; In ethanol;
DOI:10.1016/j.molstruc.2014.06.026