N¹-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-yl)-N⁸-hydroxyoctanediamide

Base Information

• Chemical Name: N¹-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-yl)-N⁸-hydroxyoctanediamide
• CAS No.: 1082051-44-2
• Molecular Formula: C₂₅H₃₀N₄O₄
• Molecular Weight: 450.538

Synonyms:N¹-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-yl)-N⁸-hydroxyoctanediamide

Chemical Property of N¹-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-yl)-N⁸-hydroxyoctanediamide

Chemical Property:

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Technology Process of N¹-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-yl)-N⁸-hydroxyoctanediamide

There total 1 articles about N¹-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-yl)-N⁸-hydroxyoctanediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoic acid (1082051-61-3) → N1-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-yl)-N8-hydroxyoctanediamide (1082051-44-2)

Guidance literature:

With O-(tert-butyldimethylsilanyl)hydroxylamine; benzotriazol-1-yloxy-tris(dimethylamino)-phosphonium chloride; triethylamine; In dichloromethane; at 20 ℃; for 20h;

DOI:10.1016/j.bmcl.2008.07.119

upstream raw materials:

8-(1,3-dimethyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-7-ylamino)-8-oxooctanoic acid

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