3-(3-Iodo-4-{(5Z,9Z,13Z,17Z,21Z,25Z,29E,33E)-6,10,14,18,22,26,30,34,38-nonamethyl-2-[(S)-4-methyl-6-triisopropylsilanyloxy-hex-(E)-ylidene]-nonatriaconta-5,9,13,17,21,25,29,33,37-nonaenyloxymethyl}-phenyl)-3-trifluoromethyl-3H-diazirine

Base Information

Chemical Name:3-(3-Iodo-4-{(5Z,9Z,13Z,17Z,21Z,25Z,29E,33E)-6,10,14,18,22,26,30,34,38-nonamethyl-2-[(S)-4-methyl-6-triisopropylsilanyloxy-hex-(E)-ylidene]-nonatriaconta-5,9,13,17,21,25,29,33,37-nonaenyloxymethyl}-phenyl)-3-trifluoromethyl-3H-diazirine
CAS No.:197968-47-1
Molecular Formula:C₇₃H₁₁₆F₃IN₂O₂Si
Molecular Weight:1265.72
Hs Code.:

3-(3-Iodo-4-{(5Z,9Z,13Z,17Z,21Z,25Z,29E,33E)-6,10,14,18,22,26,30,34,38-nonamethyl-2-[(S)-4-methyl-6-triisopropylsilanyloxy-hex-(E)-ylidene]-nonatriaconta-5,9,13,17,21,25,29,33,37-nonaenyloxymethyl}-phenyl)-3-trifluoromethyl-3H-diazirine

Synonyms:3-(3-Iodo-4-{(5Z,9Z,13Z,17Z,21Z,25Z,29E,33E)-6,10,14,18,22,26,30,34,38-nonamethyl-2-[(S)-4-methyl-6-triisopropylsilanyloxy-hex-(E)-ylidene]-nonatriaconta-5,9,13,17,21,25,29,33,37-nonaenyloxymethyl}-phenyl)-3-trifluoromethyl-3H-diazirine

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Chemical Property of 3-(3-Iodo-4-{(5Z,9Z,13Z,17Z,21Z,25Z,29E,33E)-6,10,14,18,22,26,30,34,38-nonamethyl-2-[(S)-4-methyl-6-triisopropylsilanyloxy-hex-(E)-ylidene]-nonatriaconta-5,9,13,17,21,25,29,33,37-nonaenyloxymethyl}-phenyl)-3-trifluoromethyl-3H-diazirine

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Technology Process of 3-(3-Iodo-4-{(5Z,9Z,13Z,17Z,21Z,25Z,29E,33E)-6,10,14,18,22,26,30,34,38-nonamethyl-2-[(S)-4-methyl-6-triisopropylsilanyloxy-hex-(E)-ylidene]-nonatriaconta-5,9,13,17,21,25,29,33,37-nonaenyloxymethyl}-phenyl)-3-trifluoromethyl-3H-diazirine

There total 2 articles about 3-(3-Iodo-4-{(5Z,9Z,13Z,17Z,21Z,25Z,29E,33E)-6,10,14,18,22,26,30,34,38-nonamethyl-2-[(S)-4-methyl-6-triisopropylsilanyloxy-hex-(E)-ylidene]-nonatriaconta-5,9,13,17,21,25,29,33,37-nonaenyloxymethyl}-phenyl)-3-trifluoromethyl-3H-diazirine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 197968-45-9
3-(3-Iodo-4-iodomethyl-phenyl)-3-trifluoromethyl-3H-diazirine

: (5Z,9Z,13Z,17Z,21Z,25Z,29E,33E)-6,10,14,18,22,26,30,34,38-Nonamethyl-2-[(S)-4-methyl-6-triisopropylsilanyloxy-hex-(E)-ylidene]-nonatriaconta-5,9,13,17,21,25,29,33,37-nonaen-1-ol

: 197968-47-1
3-(3-Iodo-4-{(5Z,9Z,13Z,17Z,21Z,25Z,29E,33E)-6,10,14,18,22,26,30,34,38-nonamethyl-2-[(S)-4-methyl-6-triisopropylsilanyloxy-hex-(E)-ylidene]-nonatriaconta-5,9,13,17,21,25,29,33,37-nonaenyloxymethyl}-phenyl)-3-trifluoromethyl-3H-diazirine

Guidance literature:: With sodium hydroxide; tetra-(n-butyl)ammonium iodide; In water; benzene; at 25 ℃; for 72h;
DOI:10.1021/ja9721677

Reference yield:

: 197968-46-0
[2-iodo-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]methanol

: 197968-47-1
3-(3-Iodo-4-{(5Z,9Z,13Z,17Z,21Z,25Z,29E,33E)-6,10,14,18,22,26,30,34,38-nonamethyl-2-[(S)-4-methyl-6-triisopropylsilanyloxy-hex-(E)-ylidene]-nonatriaconta-5,9,13,17,21,25,29,33,37-nonaenyloxymethyl}-phenyl)-3-trifluoromethyl-3H-diazirine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / methyltriphenylphosphonium iodide / acetonitrile / 23 h

2: aq. NaOH, tetrabutylammonium iodide / benzene; H₂O / 72 h / 25 °C

With sodium hydroxide; methyl-triphenylphosphonium iodide; tetra-(n-butyl)ammonium iodide; In water; acetonitrile; benzene;
DOI:10.1021/ja9721677