(6E,10Z,14Z,18Z,22Z,26Z,30Z,34E,38E)-(S)-7-[2-Iodo-4-(3-trifluoromethyl-3H-diazirin-3-yl)-benzyloxymethyl]-3,11,15,19,23,27,31,35,39,43-decamethyl-tetratetraconta-6,10,14,18,22,26,30,34,38,42-decaen-1-ol

Base Information

Chemical Name:(6E,10Z,14Z,18Z,22Z,26Z,30Z,34E,38E)-(S)-7-[2-Iodo-4-(3-trifluoromethyl-3H-diazirin-3-yl)-benzyloxymethyl]-3,11,15,19,23,27,31,35,39,43-decamethyl-tetratetraconta-6,10,14,18,22,26,30,34,38,42-decaen-1-ol
CAS No.:197968-33-5
Molecular Formula:C₆₄H₉₆F₃IN₂O₂
Molecular Weight:1109.38
Hs Code.:

(6E,10Z,14Z,18Z,22Z,26Z,30Z,34E,38E)-(S)-7-[2-Iodo-4-(3-trifluoromethyl-3H-diazirin-3-yl)-benzyloxymethyl]-3,11,15,19,23,27,31,35,39,43-decamethyl-tetratetraconta-6,10,14,18,22,26,30,34,38,42-decaen-1-ol

Synonyms:(6E,10Z,14Z,18Z,22Z,26Z,30Z,34E,38E)-(S)-7-[2-Iodo-4-(3-trifluoromethyl-3H-diazirin-3-yl)-benzyloxymethyl]-3,11,15,19,23,27,31,35,39,43-decamethyl-tetratetraconta-6,10,14,18,22,26,30,34,38,42-decaen-1-ol

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Chemical Property of (6E,10Z,14Z,18Z,22Z,26Z,30Z,34E,38E)-(S)-7-[2-Iodo-4-(3-trifluoromethyl-3H-diazirin-3-yl)-benzyloxymethyl]-3,11,15,19,23,27,31,35,39,43-decamethyl-tetratetraconta-6,10,14,18,22,26,30,34,38,42-decaen-1-ol

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Technology Process of (6E,10Z,14Z,18Z,22Z,26Z,30Z,34E,38E)-(S)-7-[2-Iodo-4-(3-trifluoromethyl-3H-diazirin-3-yl)-benzyloxymethyl]-3,11,15,19,23,27,31,35,39,43-decamethyl-tetratetraconta-6,10,14,18,22,26,30,34,38,42-decaen-1-ol

There total 3 articles about (6E,10Z,14Z,18Z,22Z,26Z,30Z,34E,38E)-(S)-7-[2-Iodo-4-(3-trifluoromethyl-3H-diazirin-3-yl)-benzyloxymethyl]-3,11,15,19,23,27,31,35,39,43-decamethyl-tetratetraconta-6,10,14,18,22,26,30,34,38,42-decaen-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 197968-47-1
3-(3-Iodo-4-{(5Z,9Z,13Z,17Z,21Z,25Z,29E,33E)-6,10,14,18,22,26,30,34,38-nonamethyl-2-[(S)-4-methyl-6-triisopropylsilanyloxy-hex-(E)-ylidene]-nonatriaconta-5,9,13,17,21,25,29,33,37-nonaenyloxymethyl}-phenyl)-3-trifluoromethyl-3H-diazirine

: 197968-33-5
(6E,10Z,14Z,18Z,22Z,26Z,30Z,34E,38E)-(S)-7-[2-Iodo-4-(3-trifluoromethyl-3H-diazirin-3-yl)-benzyloxymethyl]-3,11,15,19,23,27,31,35,39,43-decamethyl-tetratetraconta-6,10,14,18,22,26,30,34,38,42-decaen-1-ol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 4.5h;
DOI:10.1021/ja9721677

Reference yield:

: 197968-46-0
[2-iodo-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]methanol

: 197968-33-5
(6E,10Z,14Z,18Z,22Z,26Z,30Z,34E,38E)-(S)-7-[2-Iodo-4-(3-trifluoromethyl-3H-diazirin-3-yl)-benzyloxymethyl]-3,11,15,19,23,27,31,35,39,43-decamethyl-tetratetraconta-6,10,14,18,22,26,30,34,38,42-decaen-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / methyltriphenylphosphonium iodide / acetonitrile / 23 h

2: aq. NaOH, tetrabutylammonium iodide / benzene; H₂O / 72 h / 25 °C

3: 26.6 g / tetrabutylammonium fluoride trihydrate / tetrahydrofuran / 4.5 h

With sodium hydroxide; tetrabutyl ammonium fluoride; methyl-triphenylphosphonium iodide; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; water; acetonitrile; benzene;
DOI:10.1021/ja9721677

Reference yield:

: 197968-45-9
3-(3-Iodo-4-iodomethyl-phenyl)-3-trifluoromethyl-3H-diazirine

: 197968-33-5
(6E,10Z,14Z,18Z,22Z,26Z,30Z,34E,38E)-(S)-7-[2-Iodo-4-(3-trifluoromethyl-3H-diazirin-3-yl)-benzyloxymethyl]-3,11,15,19,23,27,31,35,39,43-decamethyl-tetratetraconta-6,10,14,18,22,26,30,34,38,42-decaen-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH, tetrabutylammonium iodide / benzene; H₂O / 72 h / 25 °C

2: 26.6 g / tetrabutylammonium fluoride trihydrate / tetrahydrofuran / 4.5 h

With sodium hydroxide; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; water; benzene;
DOI:10.1021/ja9721677