benzyl 2-methyl-4-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethylsulfonyl)butan-2-ylcarbamate

Base Information

Chemical Name:benzyl 2-methyl-4-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethylsulfonyl)butan-2-ylcarbamate
CAS No.:1373434-28-6
Molecular Formula:C₂₂H₃₇NO₈S
Molecular Weight:475.604
Hs Code.:

Synonyms:benzyl 2-methyl-4-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethylsulfonyl)butan-2-ylcarbamate

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Chemical Property of benzyl 2-methyl-4-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethylsulfonyl)butan-2-ylcarbamate

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Technology Process of benzyl 2-methyl-4-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethylsulfonyl)butan-2-ylcarbamate

There total 3 articles about benzyl 2-methyl-4-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethylsulfonyl)butan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1373434-27-5
benzyl 17-methyl-2,5,8,11-tetraoxa-14-thiaoctadecan-17-ylcarbamate

: 1373434-28-6
benzyl 2-methyl-4-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethylsulfonyl)butan-2-ylcarbamate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 2h; Product distribution / selectivity;

Reference yield:

: 187107-78-4
S-3-(benzyloxycarbonylamino)-3-methylbutyl ethanethioate

: 1373434-28-6
benzyl 2-methyl-4-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethylsulfonyl)butan-2-ylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / methanol / 1 h / 20 °C

1.2: pH ~ 5 / Cooling with ice

2.1: caesium carbonate / N,N-dimethyl-formamide / 16 h

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C

With caesium carbonate; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1226913-81-0
benzyl 4-mercapto-2-methylbutan-2-ylcarbamate

: 1373434-28-6
benzyl 2-methyl-4-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethylsulfonyl)butan-2-ylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 16 h

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C

With caesium carbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide;